9-(2-(benzyloxy)-4-(7,9-dioxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

Base Information

Chemical Name:9-(2-(benzyloxy)-4-(7,9-dioxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile
CAS No.:1428438-58-7
Molecular Formula:C₃₅H₃₁NO₇
Molecular Weight:577.634
Hs Code.:

Synonyms:9-(2-(benzyloxy)-4-(7,9-dioxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

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Chemical Property of 9-(2-(benzyloxy)-4-(7,9-dioxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

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Technology Process of 9-(2-(benzyloxy)-4-(7,9-dioxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

There total 2 articles about 9-(2-(benzyloxy)-4-(7,9-dioxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-31-6
maleic anhydride

: 1428438-97-4
C₃₃H₃₇NO₇

: 1428438-58-7
9-(2-(benzyloxy)-4-(7,9-dioxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

Guidance literature:: With acetic anhydride; acetic acid; In dichloromethane; at 140 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmc.2012.11.037

Reference yield:

: 1428438-98-5
9-(2-(benzyloxy)-4-formylphenoxy)nonanenitrile

: 1428438-58-7
9-(2-(benzyloxy)-4-(7,9-dioxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere

1.2: 3 h / -78 - 20 °C / Inert atmosphere

2.1: acetic anhydride; acetic acid / dichloromethane / 24 h / 140 °C / Inert atmosphere

With n-butyllithium; acetic anhydride; acetic acid; In tetrahydrofuran; hexane; dichloromethane; 2.1: |Diels-Alder Cycloaddition;
DOI:10.1016/j.bmc.2012.11.037