9-(2-(benzyloxy)-4-(7-oxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

Base Information

Chemical Name:9-(2-(benzyloxy)-4-(7-oxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile
CAS No.:1428438-65-6
Molecular Formula:C₃₅H₃₃NO₆
Molecular Weight:563.65
Hs Code.:

Synonyms:9-(2-(benzyloxy)-4-(7-oxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

Suppliers and Price of 9-(2-(benzyloxy)-4-(7-oxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 9-(2-(benzyloxy)-4-(7-oxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 9-(2-(benzyloxy)-4-(7-oxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

There total 3 articles about 9-(2-(benzyloxy)-4-(7-oxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428438-58-7
9-(2-(benzyloxy)-4-(7,9-dioxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

: 1428438-65-6
9-(2-(benzyloxy)-4-(7-oxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.bmc.2012.11.037

Reference yield:

: 1428438-98-5
9-(2-(benzyloxy)-4-formylphenoxy)nonanenitrile

: 1428438-65-6
9-(2-(benzyloxy)-4-(7-oxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere

1.2: 3 h / -78 - 20 °C / Inert atmosphere

2.1: acetic anhydride; acetic acid / dichloromethane / 24 h / 140 °C / Inert atmosphere

3.1: sodium tetrahydroborate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; acetic anhydride; acetic acid; In tetrahydrofuran; hexane; dichloromethane; 2.1: |Diels-Alder Cycloaddition;
DOI:10.1016/j.bmc.2012.11.037

Reference yield:

: 1428438-97-4
C₃₃H₃₇NO₇

: 1428438-65-6
9-(2-(benzyloxy)-4-(7-oxo-7,9-dihydrofuro[3',4':6,7]naphtho[1,2-d][1,3]dioxol-10-yl)phenoxy)nonanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride; acetic acid / dichloromethane / 24 h / 140 °C / Inert atmosphere

2: sodium tetrahydroborate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; acetic anhydride; acetic acid; In tetrahydrofuran; dichloromethane; 1: |Diels-Alder Cycloaddition;
DOI:10.1016/j.bmc.2012.11.037