3'-O-(1,3-benzodithiol-2-yl)-5'-O-<4,4',4''-tris(benzoyloxy)trityl>thymidine

Base Information

Chemical Name:3'-O-(1,3-benzodithiol-2-yl)-5'-O-<4,4',4''-tris(benzoyloxy)trityl>thymidine
CAS No.:86610-79-9
Molecular Formula:C₅₇H₄₄N₂O₁₁S₂
Molecular Weight:997.115
Hs Code.:

Synonyms:3'-O-(1,3-benzodithiol-2-yl)-5'-O-<4,4',4''-tris(benzoyloxy)trityl>thymidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3'-O-(1,3-benzodithiol-2-yl)-5'-O-<4,4',4''-tris(benzoyloxy)trityl>thymidine

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Technology Process of 3'-O-(1,3-benzodithiol-2-yl)-5'-O-<4,4',4''-tris(benzoyloxy)trityl>thymidine

There total 4 articles about 3'-O-(1,3-benzodithiol-2-yl)-5'-O-<4,4',4''-tris(benzoyloxy)trityl>thymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1,3-benzodithiolium tetrafluoroborate

: 86610-69-7
5'-O-<4,4',4''-tris(benzoyloxy)trityl>thymidine

: 86610-79-9
3'-O-(1,3-benzodithiol-2-yl)-5'-O-<4,4',4''-tris(benzoyloxy)trityl>thymidine

Guidance literature:: With pyridinium paratoluene sulfonic acid; In pyridine; dichloromethane; 1.) 18 h, 2.) 7 h;
DOI:10.1021/jo00166a014

Reference yield:

: 86610-67-5
4,4',4''-tris(benzoyloxy)tritylcarbinol

: 86610-79-9
3'-O-(1,3-benzodithiol-2-yl)-5'-O-<4,4',4''-tris(benzoyloxy)trityl>thymidine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / acetyl bromide / benzene / 1 h / Heating

2: 91 percent / pyridine / 2 h / 65 °C

3: 68 percent / 2.) pyridinium m-nitrobenzenesulfonate / CH₂Cl₂; pyridine / 1.) 18 h, 2.) 7 h

With Acetyl bromide; pyridinium paratoluene sulfonic acid; In pyridine; dichloromethane; benzene;
DOI:10.1021/jo00166a014

Reference yield:

: 86610-66-4
4,4',4''-tris(benzoyloxy)trityl bromide

: 86610-79-9
3'-O-(1,3-benzodithiol-2-yl)-5'-O-<4,4',4''-tris(benzoyloxy)trityl>thymidine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / pyridine / 2 h / 65 °C

2: 68 percent / 2.) pyridinium m-nitrobenzenesulfonate / CH₂Cl₂; pyridine / 1.) 18 h, 2.) 7 h

With pyridinium paratoluene sulfonic acid; In pyridine; dichloromethane;
DOI:10.1021/jo00166a014