C₆₃H₅₈O₁₅

Base Information

Chemical Name:C₆₃H₅₈O₁₅
CAS No.:1338782-86-7
Molecular Formula:C₆₃H₅₈O₁₅
Molecular Weight:1055.14
Hs Code.:

C<sub>63</sub>H<sub>58</sub>O<sub>15</sub>

Synonyms:C₆₃H₅₈O₁₅

Suppliers and Price of C₆₃H₅₈O₁₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₃H₅₈O₁₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₃H₅₈O₁₅

There total 5 articles about C₆₃H₅₈O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1338782-75-4
C₂₉H₃₂O₆

: 149707-75-5
2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl trichloroacetimidate

: 1338782-86-7
C₆₃H₅₈O₁₅

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c1cc14025f

Reference yield:

: 34212-64-1,641635-63-4
methyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside

: 1338782-86-7
C₆₃H₅₈O₁₅

Guidance literature:: Multi-step reaction with 5 steps

1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C

2: potassium carbonate / acetonitrile / Reflux

3: diethylzinc / hexane; 1,2-dichloro-ethane / 48 h / 50 °C / Molecular sieve; Inert atmosphere

4: water; potassium carbonate / methanol / 1 h / 20 °C

5: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 0 °C / Inert atmosphere

With oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; water; diethylzinc; potassium carbonate; dimethyl sulfoxide; triethylamine; In methanol; hexane; dichloromethane; 1,2-dichloro-ethane; acetonitrile; 1: Swern oxidation / 3: Simmons-Smith-Furukawa reaction;
DOI:10.1039/c1cc14025f

Reference yield:

: 342789-68-8
(E)-methyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-manno-hex-5-enopyranoside

: 1338782-86-7
C₆₃H₅₈O₁₅

Guidance literature:: Multi-step reaction with 3 steps

1: diethylzinc / hexane; 1,2-dichloro-ethane / 48 h / 50 °C / Molecular sieve; Inert atmosphere

2: water; potassium carbonate / methanol / 1 h / 20 °C

3: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 0 °C / Inert atmosphere

With trimethylsilyl trifluoromethanesulfonate; water; diethylzinc; potassium carbonate; In methanol; hexane; dichloromethane; 1,2-dichloro-ethane; 1: Simmons-Smith-Furukawa reaction;
DOI:10.1039/c1cc14025f