2-amino-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate amide

Base Information

Chemical Name:2-amino-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate amide
CAS No.:1456532-32-3
Molecular Formula:C₁₃H₁₅N₅O₅S
Molecular Weight:353.359
Hs Code.:

Synonyms:2-amino-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate amide

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Chemical Property of 2-amino-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate amide

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Technology Process of 2-amino-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate amide

There total 4 articles about 2-amino-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-30-5
succinic acid anhydride

: 1456532-36-7
2-amino-1-(4-nitro)acetophenone thiosemicarbazone

: 1456532-32-3
2-amino-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate amide

Guidance literature:: With dmap; In acetonitrile; at 20 ℃; for 48h;
DOI:10.1016/j.ejmech.2013.04.022

Reference yield:

: 99-81-0
4-Nitrophenacyl bromide

: 1456532-32-3
2-amino-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate amide

Guidance literature:: Multi-step reaction with 4 steps

1: chloroform / 24 h / 20 °C

2: hydrogenchloride / ethanol; chloroform / 72 h / 20 °C

3: acetic acid / ethanol / 24 h / 20 °C

4: dmap / acetonitrile / 48 h / 20 °C

With hydrogenchloride; dmap; acetic acid; In ethanol; chloroform; acetonitrile;
DOI:10.1016/j.ejmech.2013.04.022

Reference yield:

: 5425-81-0
2-amino-1-(4-nitrophenyl)ethanone hydrochloride

: 1456532-32-3
2-amino-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate amide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / 24 h / 20 °C

2: dmap / acetonitrile / 48 h / 20 °C

With dmap; acetic acid; In ethanol; acetonitrile;
DOI:10.1016/j.ejmech.2013.04.022