C₂₅H₃₄N₂O₂

Base Information Edit

Chemical Name:C₂₅H₃₄N₂O₂
CAS No.:1184928-27-5
Molecular Formula:C₂₅H₃₄N₂O₂
Molecular Weight:394.557
Hs Code.:
Mol file:1184928-27-5.mol

C<sub>25</sub>H<sub>34</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₅H₃₄N₂O₂

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Chemical Property of C₂₅H₃₄N₂O₂ Edit

Chemical Property:

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Technology Process of C₂₅H₃₄N₂O₂

There total 6 articles about C₂₅H₃₄N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1185253-10-4
C₂₂H₂₉NO₃

: 765-30-0
Cyclopropylamine

: 1184928-27-5
C₂₅H₃₄N₂O₂

Guidance literature:: C₂₂H₂₉NO₃; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In 2-methyltetrahydrofuran; at 0 - 10 ℃; for 0.0833333h; Industry scale;

Cyclopropylamine; In 2-methyltetrahydrofuran; at 0 - 35 ℃; for 4h; Industry scale;

Reference yield:

: 110-62-3
pentanal

: 1184928-27-5
C₂₅H₃₄N₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine / 60 h / 5 - 35 °C / Industry scale

1.2: 30 °C / Industry scale

2.1: sulfuric acid / n-heptane / 18 h / 19 - 25 °C / Industry scale; Sealed vessel

3.1: n-hexyllithium / n-heptane; tetrahydrofuran / 0.5 h / -65 - -55 °C / Industry scale

3.2: 1.5 h / -65 - -55 °C / Industry scale

4.1: (1S)-(+)-(10-camphorsulfonyl)-oxaziridine / n-heptane; tetrahydrofuran / 6 h / -65 - -55 °C / Industry scale

4.2: -60 - -40 °C / Industry scale

5.1: trifluoroacetic acid / toluene / 25.5 h / 50 °C / Industry scale

5.2: 15 - 20 °C / pH 5 - 6 / Industry scale

6.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / 2-methyltetrahydrofuran / 0.08 h / 0 - 10 °C / Industry scale

6.2: 4 h / 0 - 35 °C / Industry scale

With pyridine; n-hexyllithium; (1S)-(+)-(10-camphorsulfonyl)-oxaziridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sulfuric acid; In tetrahydrofuran; 2-methyltetrahydrofuran; n-heptane; toluene;

Reference yield:

: 18999-28-5
3-(n-Butyl)acrylic acid

: 1184928-27-5
C₂₅H₃₄N₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / n-heptane / 18 h / 19 - 25 °C / Industry scale; Sealed vessel

2.1: n-hexyllithium / n-heptane; tetrahydrofuran / 0.5 h / -65 - -55 °C / Industry scale

2.2: 1.5 h / -65 - -55 °C / Industry scale

3.1: (1S)-(+)-(10-camphorsulfonyl)-oxaziridine / n-heptane; tetrahydrofuran / 6 h / -65 - -55 °C / Industry scale

3.2: -60 - -40 °C / Industry scale

4.1: trifluoroacetic acid / toluene / 25.5 h / 50 °C / Industry scale

4.2: 15 - 20 °C / pH 5 - 6 / Industry scale

5.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / 2-methyltetrahydrofuran / 0.08 h / 0 - 10 °C / Industry scale

5.2: 4 h / 0 - 35 °C / Industry scale

With n-hexyllithium; (1S)-(+)-(10-camphorsulfonyl)-oxaziridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sulfuric acid; In tetrahydrofuran; 2-methyltetrahydrofuran; n-heptane; toluene;