Technology Process of C31H36O5
There total 6 articles about C31H36O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3-(2',3',4'-tri-O-benzyl-α-D-galactopyranosyl)-1-propene;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 0 - 20 ℃;
for 1h;
Inert atmosphere;
methyl iodide;
In
tetrahydrofuran; mineral oil;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1021/ol2032448
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: methanol; sodium methylate / 1 h / 20 °C / Inert atmosphere
2.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
3.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere
3.2: 0 - 20 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
5.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere
5.2: 0 - 20 °C / Inert atmosphere
With
1H-imidazole; methanol; tetrabutyl ammonium fluoride; sodium methylate; sodium hydride;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol2032448
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
3.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere
3.2: 0 - 20 °C / Inert atmosphere
With
tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; mineral oil;
DOI:10.1021/ol2032448
