(Z,E)-N⁶-Benzoyl-9--β-D-glycero-hepta-3,5-dienofuranosyluronate>adenine

Base Information

Chemical Name:(Z,E)-N⁶-Benzoyl-9--β-D-glycero-hepta-3,5-dienofuranosyluronate>adenine
CAS No.:85681-02-3
Molecular Formula:C₂₆H₂₇N₅O₇
Molecular Weight:521.53
Hs Code.:

(Z,E)-N<sup>6</sup>-Benzoyl-9-<ethyl 3,5,6-trideoxy-6-<3,3-(ethylenedioxy)propyl>-β-D-glycero-hepta-3,5-dienofuranosyluronate>adenine

Synonyms:(Z,E)-N⁶-Benzoyl-9--β-D-glycero-hepta-3,5-dienofuranosyluronate>adenine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z,E)-N⁶-Benzoyl-9--β-D-glycero-hepta-3,5-dienofuranosyluronate>adenine

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Technology Process of (Z,E)-N⁶-Benzoyl-9--β-D-glycero-hepta-3,5-dienofuranosyluronate>adenine

There total 7 articles about (Z,E)-N⁶-Benzoyl-9--β-D-glycero-hepta-3,5-dienofuranosyluronate>adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 85681-01-2
(E)-N⁶-Benzoyl-9--2,3-O-isopropylidene-β-D-ribo-hept-5-eno-furanosyluronate>adenine

: 85681-02-3
(Z,E)-N⁶-Benzoyl-9--β-D-glycero-hepta-3,5-dienofuranosyluronate>adenine

Guidance literature:: With sodium ethanolate; In ethanol; for 4h; Ambient temperature;
DOI:10.1021/jo00160a008

Reference yield:

: 38049-07-9
1,3-Dioxolan-2-buttersaeure-ethylester

: 85681-02-3
(Z,E)-N⁶-Benzoyl-9--β-D-glycero-hepta-3,5-dienofuranosyluronate>adenine

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / cyclohexylisopropylamine, n-butyllithium, iodine / tetrahydrofuran / 0.25 h / -78 °C

2: 59 percent / tetrahydrothiophene 1,1-dioxide / 4 h / 60 °C

3: 90 percent / potassium tert-butoxide / CH₂Cl₂; acetonitrile; benzene / 1 h / 40 °C

4: 56 percent / sodium ethoxide / ethanol / 4 h / Ambient temperature

With n-butyllithium; N-cyclohexylisopropylamine; potassium tert-butylate; iodine; sodium ethanolate; In tetrahydrofuran; sulfolane; ethanol; dichloromethane; acetonitrile; benzene;
DOI:10.1021/jo00160a008

Reference yield:

: 43077-06-1
6-N-benzoyl-2',3'-O-isopropylideneadenosine-5'-aldehyde

: 85681-02-3
(Z,E)-N⁶-Benzoyl-9--β-D-glycero-hepta-3,5-dienofuranosyluronate>adenine

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / acetonitrile / 0.25 h / Ambient temperature

2: 56 percent / sodium ethoxide / ethanol / 4 h / Ambient temperature

With sodium ethanolate; In ethanol; acetonitrile;
DOI:10.1021/jo00160a008