Diethyl [2-(1,3-dioxolan-2-yl)ethyl]propanedioate

Base Information Edit

Chemical Name:Diethyl [2-(1,3-dioxolan-2-yl)ethyl]propanedioate
CAS No.:23985-06-0
Molecular Formula:C12H20 O6
Molecular Weight:260.287
Hs Code.:
NSC Number:19889
DSSTox Substance ID:DTXSID50281049
Nikkaji Number:J1.622.019A
Wikidata:Q82014782
Mol file:23985-06-0.mol

Synonyms:23985-06-0;NSC19889;diethyl [2-(1,3-dioxolan-2-yl)ethyl]propanedioate;DTXSID50281049;NSC-19889;AKOS004907159;diethyl [2-(1,3-dioxolan-2-yl)ethyl]malonate

Suppliers and Price of Diethyl [2-(1,3-dioxolan-2-yl)ethyl]propanedioate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Diethyl [2-(1,3-dioxolan-2-yl)ethyl]propanedioate Edit

Chemical Property:

Vapor Pressure:0.000384mmHg at 25°C
Boiling Point:317.5°Cat760mmHg
Flash Point:135.6°C
Density:1.125g/cm³
XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:9
Exact Mass:260.12598835
Heavy Atom Count:18
Complexity:254

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(CCC1OCCO1)C(=O)OCC

Technology Process of Diethyl [2-(1,3-dioxolan-2-yl)ethyl]propanedioate

There total 4 articles about Diethyl [2-(1,3-dioxolan-2-yl)ethyl]propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 19515-61-8
diethyl 2-(3-oxo-propyl)malonate

: 107-21-1
ethylene glycol

: 23985-06-0
Ethyl 2-ethoxycarbonyl-4-(1',3'-dioxolan-2'-yl)butanoate

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 24h; Heating;
DOI:10.1248/cpb.41.339

Reference yield: 73.0%

: 18742-02-4
2-bromo-2-(2-ethyl)dioxolane

: 105-53-3
diethyl malonate

: 23985-06-0
Ethyl 2-ethoxycarbonyl-4-(1',3'-dioxolan-2'-yl)butanoate

Guidance literature:: diethyl malonate; With sodium ethanolate; In ethanol; at 55 ℃;

2-bromo-2-(2-ethyl)dioxolane; In ethanol; at 55 ℃; for 0.416667h;
DOI:10.1055/s-2000-8223