(Benzyl-2,3,4-tri-O-benzyl-α-D-glucopyranosid-6)-(2,2,2-trichlorethyl)-(triethylammonium)-phosphat

Base Information

• Chemical Name: (Benzyl-2,3,4-tri-O-benzyl-α-D-glucopyranosid-6)-(2,2,2-trichlorethyl)-(triethylammonium)-phosphat
• CAS No.: 112104-67-3
• Molecular Formula: C₆H₁₅N*C₃₆H₃₈Cl₃O₉P
• Molecular Weight: 853.217
• Mol file: 112104-67-3.mol

Synonyms:(Benzyl-2,3,4-tri-O-benzyl-α-D-glucopyranosid-6)-(2,2,2-trichlorethyl)-(triethylammonium)-phosphat

Chemical Property of (Benzyl-2,3,4-tri-O-benzyl-α-D-glucopyranosid-6)-(2,2,2-trichlorethyl)-(triethylammonium)-phosphat

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of (Benzyl-2,3,4-tri-O-benzyl-α-D-glucopyranosid-6)-(2,2,2-trichlorethyl)-(triethylammonium)-phosphat

There total 1 articles about (Benzyl-2,3,4-tri-O-benzyl-α-D-glucopyranosid-6)-(2,2,2-trichlorethyl)-(triethylammonium)-phosphat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

benzyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside (59935-49-8) + 2,2,2-trichloroethyl phosphorodichloridate (18868-46-7) → (Benzyl-2,3,4-tri-O-benzyl-α-D-glucopyranosid-6)-(2,2,2-trichlorethyl)-(triethylammonium)-phosphat (112104-67-3)

Guidance literature:

With 1,2,4-Triazole; In pyridine; for 0.25h; Ambient temperature;

DOI:10.1016/0008-6215(86)84003-4

Reference yield: 83.0%

benzyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside (59935-49-8) + (Benzyl-2,3,4-tri-O-benzyl-α-D-glucopyranosid-6)-(2,2,2-trichlorethyl)-(triethylammonium)-phosphat (112104-67-3) → -(2,2,2-trichlorethyl)-phosphat (112104-85-5)

Guidance literature:

With 1-Mesitylensulfonsaeure-<1H>-3-nitrotriazol; In pyridine; for 0.75h; Ambient temperature;

DOI:10.1016/0008-6215(86)84003-4

upstream raw materials:

benzyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside

2,2,2-trichloroethyl phosphorodichloridate

Downstream raw materials:

-(2,2,2-trichlorethyl)-phosphat