{Ta(S-2,4,6-C6H2-i-Pr3)3(THF)}2(μ-N2)

Base Information

• Chemical Name: {Ta(S-2,4,6-C6H2-i-Pr3)3(THF)}2(μ-N2)
• CAS No.: 114198-89-9
• Molecular Formula: C₉₈H₁₅₄N₂O₂S₆Ta₂
• Molecular Weight: 1946.6

Synonyms:{Ta(S-2,4,6-C6H2-i-Pr3)3(THF)}2(μ-N2)

Chemical Property of {Ta(S-2,4,6-C6H2-i-Pr3)3(THF)}2(μ-N2)

Chemical Property:

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Technology Process of {Ta(S-2,4,6-C6H2-i-Pr3)3(THF)}2(μ-N2)

There total 1 articles about {Ta(S-2,4,6-C6H2-i-Pr3)3(THF)}2(μ-N2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

{TaCl3(THF)2}2(μ-N2) (90130-65-7) + sodium 2,4,6-triisopropylbenzenethiolate → {Ta(S-2,4,6-C6H2-i-Pr3)3(THF)}2(μ-N2) (114198-89-9)

Guidance literature:

In diethyl ether; NaS-2,4,6-C6H2-i-Pr3 was added to a suspn. of {TaCl3(THF)2}2(μ-N2) in ether at room temperature. The react. mixt. was stirred at room temp. for 2 h.; The react. mixt. was filtered, and the solvent was removed from the filtrate in vacuo. The residue was dissolved in pentane and the soln. cooled to -30°C. to give crystals. Elem.anal.;

Reference yield: 25.0%

{Ta(S-2,4,6-C6H2-i-Pr3)3(THF)}2(μ-N2) (114198-89-9) + benzaldehyde (100-52-7) → benzaldehyde azine (588-68-1,28867-76-7,65997-87-7,65997-88-8)

Guidance literature:

In benzene-d6; {Ta(S-2,4,6-C6H2-i-Pr3)3(THF)}2(μ-N2) was dissolved in benzene-d6, and benzaldehyde was added. Further products.; The react. was monitored by (1)H-NMR spectroscopy.;

upstream raw materials:

{TaCl3(THF)2}2(μ-N2)

Downstream raw materials:

benzaldehyde azine

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