2-(benzo[1,2,5]thiadiazole-4-sulfonylamino)-4,5-dichlorobenzoyl chloride

Base Information

Chemical Name:2-(benzo[1,2,5]thiadiazole-4-sulfonylamino)-4,5-dichlorobenzoyl chloride
CAS No.:1297599-49-5
Molecular Formula:C₁₃H₆Cl₃N₃O₃S₂
Molecular Weight:422.7
Hs Code.:

Synonyms:2-(benzo[1,2,5]thiadiazole-4-sulfonylamino)-4,5-dichlorobenzoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(benzo[1,2,5]thiadiazole-4-sulfonylamino)-4,5-dichlorobenzoyl chloride

Chemical Property:

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Technology Process of 2-(benzo[1,2,5]thiadiazole-4-sulfonylamino)-4,5-dichlorobenzoyl chloride

There total 9 articles about 2-(benzo[1,2,5]thiadiazole-4-sulfonylamino)-4,5-dichlorobenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 880347-55-7
2-(benzo[1,2,5]thiadiazole-4-sulfonylamino)-4,5-dichlorobenzoic acid

: 1297599-49-5
2-(benzo[1,2,5]thiadiazole-4-sulfonylamino)-4,5-dichlorobenzoyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1039/c0ob01004a

Reference yield:

: 60695-93-4
methyl 4,5-dichloro-2-(chlorocarbonyl)benzoate

: 1297599-49-5
2-(benzo[1,2,5]thiadiazole-4-sulfonylamino)-4,5-dichlorobenzoyl chloride

Guidance literature:: Multi-step reaction with 5 steps

1: sodium azide / water; acetone

2: water; acetic acid

3: pyridine / dichloromethane

4: water; lithium hydroxide / tetrahydrofuran

5: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 16 h / 20 °C

With pyridine; sodium azide; oxalyl dichloride; water; acetic acid; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c0ob01004a

Reference yield:

: C₈H₅Cl₂N₃O₂

: 1297599-49-5
2-(benzo[1,2,5]thiadiazole-4-sulfonylamino)-4,5-dichlorobenzoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: water; acetic acid

2: pyridine / dichloromethane

3: water; lithium hydroxide / tetrahydrofuran

4: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 16 h / 20 °C

With pyridine; oxalyl dichloride; water; acetic acid; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c0ob01004a