n-butyl 9-fluoro-2-methyl-5-phenylpyrazolo[5,1-a]isoquinoline-1-carboxylate

Base Information

Chemical Name:n-butyl 9-fluoro-2-methyl-5-phenylpyrazolo[5,1-a]isoquinoline-1-carboxylate
CAS No.:1367861-17-3
Molecular Formula:C₂₃H₂₁FN₂O₂
Molecular Weight:376.43
Hs Code.:

Synonyms:n-butyl 9-fluoro-2-methyl-5-phenylpyrazolo[5,1-a]isoquinoline-1-carboxylate

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Chemical Property of n-butyl 9-fluoro-2-methyl-5-phenylpyrazolo[5,1-a]isoquinoline-1-carboxylate

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Technology Process of n-butyl 9-fluoro-2-methyl-5-phenylpyrazolo[5,1-a]isoquinoline-1-carboxylate

There total 2 articles about n-butyl 9-fluoro-2-methyl-5-phenylpyrazolo[5,1-a]isoquinoline-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1188447-26-8
n-butyl buta-2,3-dienoate

: 1353561-06-4
C₂₂H₁₇FN₂O₂S

: 1367861-17-3
n-butyl 9-fluoro-2-methyl-5-phenylpyrazolo[5,1-a]isoquinoline-1-carboxylate

Guidance literature:: With triphenylphosphine; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; at 60 ℃; Air atmosphere;
DOI:10.1016/j.tet.2012.02.013

Reference yield:

: 1112200-15-3
C₂₂H₁₇FN₂O₂S

: 1367861-17-3
n-butyl 9-fluoro-2-methyl-5-phenylpyrazolo[5,1-a]isoquinoline-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: silver trifluoromethanesulfonate / 1,2-dichloro-ethane / 1 h / 55 °C / Air atmosphere

2: triphenylphosphine / 1,2-dichloro-ethane; N,N-dimethyl-formamide / 60 °C / Air atmosphere

With silver trifluoromethanesulfonate; triphenylphosphine; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.02.013