4-methyl-d3-benzyl alcohol

Base Information

Chemical Name:4-methyl-d3-benzyl alcohol
CAS No.:78585-67-8
Molecular Formula:C₈H₁₀O
Molecular Weight:125.143
Hs Code.:

Synonyms:4-methyl-d3-benzyl alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-d3-benzyl alcohol

Chemical Property:

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Technology Process of 4-methyl-d3-benzyl alcohol

There total 5 articles about 4-methyl-d3-benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 19215-16-8
p-trideuteromethylbenzoic acid

: 78585-67-8
4-methyl-d3-benzyl alcohol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at -20 - 20 ℃; for 5h;
DOI:10.1021/ja0656604

Reference yield: 61.9%

: 19315-35-6
ethyl 4-methyl-d3-benzoate

: 78585-67-8
4-methyl-d3-benzyl alcohol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1021/ja00411a007

Reference yield:

: 619-42-1
4-methoxycarbonylphenyl bromide

: 78585-67-8
4-methyl-d3-benzyl alcohol

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / lithium tetradeuterioaluminate / tetrahydrofuran / 1.5 h

2: 96 percent / phosphorus tribromode / diethyl ether / 1.) 2 h; 2.) reflux, 2 h

3: 53 percent / lithium tetradeuterioaluminate / tetrahydrofuran / 1.) 45 min, 2.) reflux, 3 h

4: 37 percent / 1.) magnesium / 1.) ethyl ether, 0.5 h, 2.) reflux, 0.5 h

5: 61.9 percent / lithium tetrahydroaluminate / tetrahydrofuran

With lithium aluminium tetrahydride; lithium aluminium deuteride; phosphorus tribromide; magnesium; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00411a007