methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-nitro-β-D-erythro-hex-2-enopyranoside

Base Information

Chemical Name:methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-nitro-β-D-erythro-hex-2-enopyranoside
CAS No.:25541-58-6
Molecular Formula:C₁₄H₁₅NO₆
Molecular Weight:293.276
Hs Code.:

Synonyms:methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-nitro-β-D-erythro-hex-2-enopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-nitro-β-D-erythro-hex-2-enopyranoside

Chemical Property:

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Technology Process of methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-nitro-β-D-erythro-hex-2-enopyranoside

There total 2 articles about methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-nitro-β-D-erythro-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74720-67-5
C₁₄H₁₆⁽²⁾HNO₆

: 25541-58-6
methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-nitro-β-D-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: BuLi / tetrahydrofuran / 0 °C

2: 35 percent aq. H₂O₂ / tetrahydrofuran

With n-butyllithium; dihydrogen peroxide; In tetrahydrofuran;
DOI:10.1039/c39810000261

Reference yield:

: 25541-58-6
methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-nitro-β-D-erythro-hex-2-enopyranoside

Guidance literature:: Methyl-2-O-acetyl-4,6-O-benzyliden-3-deoxy-3-nitro-β-O-mannopyranosid, Natriumbicarbonat, Benzol (Erwaermen);
DOI:10.1139/v65-240

Reference yield: 95.0%

: 25541-58-6
methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-nitro-β-D-erythro-hex-2-enopyranoside

: 824-79-3,7257-26-3
p-toluenesulfinic acid sodium salt dihydrate

: 111614-23-4
methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-nitro-2-C-p-tolylsulfonyl-β-D-glucopyranoside

Guidance literature:: cetyltributylphosphonium bromide; In water; acetic acid; benzene; for 4h; Ambient temperature;
DOI:10.1016/0008-6215(87)80250-1