METHYL-4,6-O-BENZYLIDENE-3-DEOXY-3-NITRO-BETA-D-GLUCOPYRANOSIDE

Base Information

Chemical Name:METHYL-4,6-O-BENZYLIDENE-3-DEOXY-3-NITRO-BETA-D-GLUCOPYRANOSIDE
CAS No.:25541-57-5
Molecular Formula:C₁₄H₁₇NO₇
Molecular Weight:311.291
Hs Code.:
Mol file:25541-57-5.mol

Synonyms:Glucopyranoside,methyl 4,6-O-benzylidene-3-deoxy-3-nitro-, b-D- (8CI); Pyrano[3,2-d]-1,3-dioxin, b-D-glucopyranoside deriv.; Durrin

Suppliers and Price of METHYL-4,6-O-BENZYLIDENE-3-DEOXY-3-NITRO-BETA-D-GLUCOPYRANOSIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of METHYL-4,6-O-BENZYLIDENE-3-DEOXY-3-NITRO-BETA-D-GLUCOPYRANOSIDE

Chemical Property:

Boiling Point:510.8±50.0 °C(Predicted)
PKA:3.27±0.70(Predicted)
PSA：102.97000
Density:1.40±0.1 g/cm3(Predicted)
LogP:1.00130

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of METHYL-4,6-O-BENZYLIDENE-3-DEOXY-3-NITRO-BETA-D-GLUCOPYRANOSIDE

There total 5 articles about METHYL-4,6-O-BENZYLIDENE-3-DEOXY-3-NITRO-BETA-D-GLUCOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.2%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 25541-58-6
methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-nitro-β-D-erythro-hex-2-enopyranoside

: 25541-57-5
Methyl-(4,6-O-benzyliden-3-desoxy-3-nitro-β-D-glucopyranosid)

: 66101-30-2
methyl 4,6-O-benzylidene-2-deoxy-β-D-erythro-hexopyranosid-3-ulose

: methyl 4,6-O-benzylidene-2,3-dideoxy-3-nitro-2-C-<(S)-tetrahydrofuran-2-yl>-β-D-glucopyranoside

: methyl 4,6-O-benzylidene-2,3-dideoxy-3-nitro-2-C-<(R)-tetrahydrofuran-2-yl>-β-D-glucopyranoside

: 112472-90-9,112472-91-0,112472-93-2
methyl 4,6-O-benzylidene-2,3-dideoxy-3-nitro-2-C-<(S)-tetrahydrofuran-2-yl>-β-D-mannopyranoside

Guidance literature:: at 24 ℃; for 8h; Product distribution; Mechanism; Irradiation; stereoselectivity studied; also at 60 deg C; effect of additives;
DOI:10.1016/0008-6215(87)80184-2