TiCl₄*1,2-DME

Base Information

Chemical Name:TiCl₄*1,2-DME
CAS No.:19289-17-9
Molecular Formula:C₄H₁₀O₂*Cl₄Ti
Molecular Weight:279.814
Hs Code.:

Synonyms:TiCl₄*1,2-DME

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of TiCl₄*1,2-DME

Chemical Property:

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Technology Process of TiCl₄*1,2-DME

There total 1 articles about TiCl₄*1,2-DME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: NbOCl₃(1,2-dimethoxyethane)

: 7550-45-0
titanium tetrachloride

: 19289-17-9
TiCl₄(DME)

: 13597-20-1
niobium(V) oxychloride

Guidance literature:: In dichloromethane; (under Ar, Schlenk); Nb-complex added to CH2Cl2, treated with TiCl4; dried under vac,, dissolved in CDCl3 and CH2Cl2, layered with pentane, 24 h at room temp.; elem. anal.;
DOI:10.1039/b810210d

Reference yield: 88.0%

: 4-(3-(2,3,5-trimethylcyclopentadienyl)-4-(cyclohexylamido)benzyl)-2-(2,3,5-tri-methylcyclopentadienyl)-N-cyclohexylbenzeneamido tetralithium salt

: 19289-17-9
TiCl₄(DME)

: 917-54-4
methyllithium

: methylidene-bis(3,4-phenylene(cyclohexylamido)(2,3,5-trimethylcyclopentadienyl)titanium dimethyl)

Guidance literature:: In diethyl ether; at -30 - 20 ℃; for 3.25h;

Reference yield:

: 19289-17-9
TiCl₄*1,2-DME

: 917-54-4
methyllithium

: 35739-70-9
dimethyldichlorotitanium(IV)

Guidance literature:: In tetrahydrofuran; diethyl ether; Ar-atmosphere; addn. of MeLi (2 equivs., Et2O soln.) to soln. of Ti-compound at 0°C, stirring for 15 min; not sepd.;
DOI:10.1021/om9902380