N'-(trans-4{[4-(furo[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}cyclohexyl)-N,N-dimethylsulfamide

Base Information

Chemical Name:N'-(trans-4{[4-(furo[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}cyclohexyl)-N,N-dimethylsulfamide
CAS No.:1352737-36-0
Molecular Formula:C₂₁H₃₃N₅O₃S
Molecular Weight:435.591
Hs Code.:

Synonyms:N'-(trans-4{[4-(furo[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}cyclohexyl)-N,N-dimethylsulfamide

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Chemical Property of N'-(trans-4{[4-(furo[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}cyclohexyl)-N,N-dimethylsulfamide

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Technology Process of N'-(trans-4{[4-(furo[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}cyclohexyl)-N,N-dimethylsulfamide

There total 4 articles about N'-(trans-4{[4-(furo[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}cyclohexyl)-N,N-dimethylsulfamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: trans-4-[2-(4-furo[3,2-c]pyridin-4-yl-piperazin-1-yl)-ethyl]-cyclohexylamine trihydrochloride

: 13360-57-1
dimethylamino sulfonyl chloride

: 1352737-36-0
N'-(trans-4{[4-(furo[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}cyclohexyl)-N,N-dimethylsulfamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 81078-84-4
4-(1-piperazinyl)furo<3,2-c>pyridine

: 1352737-36-0
N'-(trans-4{[4-(furo[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}cyclohexyl)-N,N-dimethylsulfamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,2-dichloro-ethane; methanol / 8 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C

2.1: hydrogenchloride / ethyl acetate; methanol / 20 °C

3.1: triethylamine / dichloromethane / 0 - 20 °C

With hydrogenchloride; triethylamine; In methanol; dichloromethane; ethyl acetate; 1,2-dichloro-ethane;

Reference yield:

: 1352737-05-3
trans-{4-[2-(4-furo[3,2-c]pyridin-4-yl-piperazin-1-yl)-ethyl]-cyclohexyl}-carbamic acid tert-butyl ester

: 1352737-36-0
N'-(trans-4{[4-(furo[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}cyclohexyl)-N,N-dimethylsulfamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethyl acetate; methanol / 20 °C

2: triethylamine / dichloromethane / 0 - 20 °C

With hydrogenchloride; triethylamine; In methanol; dichloromethane; ethyl acetate;