Technology Process of C25H36O4
There total 5 articles about C25H36O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
at 0 - 20 ℃;
DOI:10.1021/ol005913c
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 80 percent / CrO3; H2SO4 / acetone; H2O / 0 °C
2.1: ZnCl2; hydroquinone / diethyl ether / 72 h / Heating
2.2: acetic acid / diethyl ether; H2O / 3 h / 20 °C
2.3: sodium methoxide / methanol / 24 h / Heating
3.1: p-toluenesulfonic acid / 5 h / Heating
4.1: 1.85 g / Oxone; NaHCO3 / acetone; H2O / 3 h
5.1: trimethylsilyl triflate / CH2Cl2 / 10 h / 0 - 20 °C
With
chromium(VI) oxide; Oxone; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; sodium hydrogencarbonate; toluene-4-sulfonic acid; hydroquinone; zinc(II) chloride;
In
diethyl ether; dichloromethane; water; acetone;
2.3: intramolecular aldol reaction;
DOI:10.1021/jo051212n
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ZnCl2; hydroquinone / diethyl ether / 72 h / Heating
1.2: acetic acid / diethyl ether; H2O / 3 h / 20 °C
1.3: sodium methoxide / methanol / 24 h / Heating
2.1: p-toluenesulfonic acid / 5 h / Heating
3.1: 1.85 g / Oxone; NaHCO3 / acetone; H2O / 3 h
4.1: trimethylsilyl triflate / CH2Cl2 / 10 h / 0 - 20 °C
With
Oxone; trimethylsilyl trifluoromethanesulfonate; sodium hydrogencarbonate; toluene-4-sulfonic acid; hydroquinone; zinc(II) chloride;
In
diethyl ether; dichloromethane; water; acetone;
1.3: intramolecular aldol reaction;
DOI:10.1021/jo051212n
