(N-ethyl-5,10,15,20-tetraphenylporphinato)copper(II) trifluoromethanesulfonate

Base Information

Chemical Name:(N-ethyl-5,10,15,20-tetraphenylporphinato)copper(II) trifluoromethanesulfonate
CAS No.:92396-64-0
Molecular Formula:CF₃O₃S*C₄₆H₃₃CuN₄
Molecular Weight:854.411
Hs Code.:

Synonyms:(N-ethyl-5,10,15,20-tetraphenylporphinato)copper(II) trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (N-ethyl-5,10,15,20-tetraphenylporphinato)copper(II) trifluoromethanesulfonate

Chemical Property:

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Technology Process of (N-ethyl-5,10,15,20-tetraphenylporphinato)copper(II) trifluoromethanesulfonate

There total 1 articles about (N-ethyl-5,10,15,20-tetraphenylporphinato)copper(II) trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: copper(II) bis(trifluoromethanesulfonate) hexahydrate

: N-ethyl-5,10,15,20-tetraphenylporphyrin

: 14172-91-9
5,10,15,20-tetraphenylporphyrin Cu(II) complex

: 92396-64-0
(N-ethyl-5,10,15,20-tetraphenylporphinato)copper(II) trifluoromethanesulfonate

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine; In acetonitrile; ligand was dissolved in dry CH3CN containing 3-fold excess of Cu salt, 2,2,6,6-tetramethylpiperidine was added, stirred for 1 h; filtered, evapd. by rotary evapn., washed with water, extd. into CH2Cl2, dried over Na2SO4, purified by flash chromy. with 2-3% MeOH in CH2Cl2 as eluent, recovered by flash rotary evaporator , stored in freezer; elem. anal.;

Reference yield:

: 92396-64-0
(N-ethyl-5,10,15,20-tetraphenylporphinato)copper(II) trifluoromethanesulfonate

: 111-92-2
dibutylamine

: 14172-91-9
5,10,15,20-tetraphenylporphyrin Cu(II) complex

Guidance literature:: In acetonitrile; byproducts: di-n-butylethylamine; 2-fold excess of (n-Bu)2NH, 2.5 d at 30-45°C, soln. was made alkaline with solid NaOH; monitored spectrophotometrically; Kinetics;