[2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

Base Information

• Chemical Name: [2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane
• CAS No.: 955094-70-9
• Molecular Formula: C₃₅H₂₃Cl₈N
• Molecular Weight: 741.198

Synonyms:[2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

Chemical Property of [2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

Chemical Property:

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Technology Process of [2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

There total 7 articles about [2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

[2,6-dichloro-4-(3,6-diacetyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane (955094-71-0) → [2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane (955094-70-9)

Guidance literature:

With hydrogenchloride; mercury dichloride; zinc; In toluene; for 24h; Heating;

DOI:10.1021/jo0708846

Reference yield: 35.0%

[2,6-dichloro-4-(3,6-diacetyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl (955094-77-6) → [2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane (955094-70-9)

Guidance literature:

With hydrogenchloride; mercury dichloride; zinc; In toluene; for 48h; Heating;

DOI:10.1021/jo0708846

Reference yield: 17.0%

3,6-diethyl-9H-carbazole (849820-61-7) + tris(2,4,6‐trichlorophenyl)methyl radical (109745-46-2) → [2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane (955094-70-9) + tris(2,4,6-trichlorophenyl)methane (105633-27-0)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; for 2h; Heating;

DOI:10.1021/jo0708846

upstream raw materials:

[2,6-dichloro-4-(3,6-diacetyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

[2,6-dichloro-4-(3,6-diacetyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

3,6-diethyl-9H-carbazole

tris(2,4,6‐trichlorophenyl)methyl radical

Downstream raw materials:

[2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

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