[2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

Base Information

Chemical Name:[2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl
CAS No.:955094-76-5
Molecular Formula:C₃₅H₂₂Cl₈N
Molecular Weight:740.19
Hs Code.:

Synonyms:[2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

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Chemical Property of [2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

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Technology Process of [2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

There total 6 articles about [2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 955094-70-9
[2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane

: 955094-76-5
[2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

Guidance literature:: [2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methane; With tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; hexane; at 20 ℃; for 5h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; hexane; for 2h; Further stages.;
DOI:10.1021/jo0708846

Reference yield:

: 881917-50-6
[4-(N-carbazolyl)-2,6-dichlorophenyl]bis(2,4,6-trichlorophenyl)methane

: 955094-76-5
[2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

Guidance literature:: Multi-step reaction with 3 steps

1.1: 80 percent / AlCl₃ / CS₂ / 2 h / Heating

2.1: 71 percent / Zn; HgCl₂; aq. HCl / toluene / 24 h / Heating

3.1: tetrabutylammonium hydroxide / hexane; tetrahydrofuran / 5 h / 20 °C

3.2: 52 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / hexane; tetrahydrofuran / 2 h

With hydrogenchloride; aluminium trichloride; tetra(n-butyl)ammonium hydroxide; mercury dichloride; zinc; In tetrahydrofuran; carbon disulfide; hexane; toluene; 1.1: Friedel-Crafts reaction / 2.1: Clemmensen reduction;
DOI:10.1021/jo0708846

Reference yield:

: 881917-48-2
(4-(N-carbazolyl)-2,6-dichlorophenyl)bis(2,4,6-trichlorophenyl)methyl radical

: 955094-76-5
[2,6-dichloro-4-(3,6-diethyl-N-carbazolyl)phenyl]bis(2,4,6-trichlorophenyl)methyl

Guidance literature:: Multi-step reaction with 3 steps

1.1: 89 percent / AlCl₃ / CS₂ / 2 h / Heating

2.1: 35 percent / Zn; HgCl₂; aq. HCl / toluene / 48 h / Heating

3.1: tetrabutylammonium hydroxide / hexane; tetrahydrofuran / 5 h / 20 °C

3.2: 52 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / hexane; tetrahydrofuran / 2 h

With hydrogenchloride; aluminium trichloride; tetra(n-butyl)ammonium hydroxide; mercury dichloride; zinc; In tetrahydrofuran; carbon disulfide; hexane; toluene; 1.1: Friedel-Crafts reaction / 2.1: Clemmensen reduction;
DOI:10.1021/jo0708846