N-(2,2-dichloro-3-(4-chlorophenyl)-3-oxo-1-phenylpropyl)phenylsulfonamide

Base Information

Chemical Name:N-(2,2-dichloro-3-(4-chlorophenyl)-3-oxo-1-phenylpropyl)phenylsulfonamide
CAS No.:907563-75-1
Molecular Formula:C₂₁H₁₆Cl₃NO₃S
Molecular Weight:468.788
Hs Code.:

Synonyms:N-(2,2-dichloro-3-(4-chlorophenyl)-3-oxo-1-phenylpropyl)phenylsulfonamide

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Chemical Property of N-(2,2-dichloro-3-(4-chlorophenyl)-3-oxo-1-phenylpropyl)phenylsulfonamide

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Technology Process of N-(2,2-dichloro-3-(4-chlorophenyl)-3-oxo-1-phenylpropyl)phenylsulfonamide

There total 4 articles about N-(2,2-dichloro-3-(4-chlorophenyl)-3-oxo-1-phenylpropyl)phenylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 907563-69-3
N-[(3E)-2,2-dichloro-3-(4-chlorophenyl)-3-(isopropylimino)-1-phenylpropyl]phenylsulfonamide

: 907563-75-1
N-(2,2-dichloro-3-(4-chlorophenyl)-3-oxo-1-phenylpropyl)phenylsulfonamide

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 14h;
DOI:10.1021/jo060241a

Reference yield:

: 98-10-2
benzenesulfonamide

: 907563-75-1
N-(2,2-dichloro-3-(4-chlorophenyl)-3-oxo-1-phenylpropyl)phenylsulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 170 °C

2.1: lithium diisopropylamide / tetrahydrofuran; hexane / 0.5 h / 0 °C

2.2: tetrahydrofuran; hexane / 14 h / -40 - 20 °C

3.1: 95 percent / HCl / tetrahydrofuran; H₂O / 14 h / 20 °C

With hydrogenchloride; lithium diisopropyl amide; In tetrahydrofuran; hexane; water;
DOI:10.1021/jo060241a

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 907563-75-1
N-(2,2-dichloro-3-(4-chlorophenyl)-3-oxo-1-phenylpropyl)phenylsulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 170 °C

2.1: lithium diisopropylamide / tetrahydrofuran; hexane / 0.5 h / 0 °C

2.2: tetrahydrofuran; hexane / 14 h / -40 - 20 °C

3.1: 95 percent / HCl / tetrahydrofuran; H₂O / 14 h / 20 °C

With hydrogenchloride; lithium diisopropyl amide; In tetrahydrofuran; hexane; water;
DOI:10.1021/jo060241a