5Z-cyclodecen-1-one

Base Information

• Chemical Name: 5Z-cyclodecen-1-one
• CAS No.: 3468-78-8
• Molecular Formula: C₁₀H₁₆O
• Molecular Weight: 152.236
• Mol file: 3468-78-8.mol

Synonyms:5Z-cyclodecen-1-one

Chemical Property of 5Z-cyclodecen-1-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5Z-cyclodecen-1-one

There total 3 articles about 5Z-cyclodecen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

trans-2-(4-iodobutyl)-3-tributylstannylcyclohexanone (120596-52-3) → 5Z-cyclodecen-1-one (3468-78-8) + 2-butylcyclohex-2-en-1-one (34737-39-8) + trans-5-cyclodecenone (3468-77-7)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 2h; Yields of byproduct given. Title compound not separated from byproducts; Heating;

DOI:10.1016/0040-4020(89)80003-1

Reference yield: 33.0%

trans-2-(4-phenylselenobutyl)-3-tributylstannylcyclohexanone (120596-56-7,120596-67-0) → 5Z-cyclodecen-1-one (3468-78-8) + 2-butylcyclohex-2-en-1-one (34737-39-8) + trans-5-cyclodecenone (3468-77-7)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 24h; Title compound not separated from byproducts; Heating;

DOI:10.1016/0040-4020(89)80003-1

Reference yield:

1Z,5E-cyclodecadiene (1124-78-3) → 5Z-cyclodecen-1-one (3468-78-8) + 1Z,6Z-cyclodecadiene (1124-79-4)

Guidance literature:

With water; oxygen; copper(l) chloride; palladium dichloride; In tetrahydrofuran; at 60 ℃; Yield given. Yields of byproduct given;

DOI:10.1007/BF00953862

upstream raw materials:

1Z,5E-cyclodecadiene

trans-2-(4-iodobutyl)-3-tributylstannylcyclohexanone

trans-2-(4-phenylselenobutyl)-3-tributylstannylcyclohexanone

Downstream raw materials:

cyclodecanone