3-IODO-5,7-DIMETHYL (1H)INDAZOLE

Base Information

Chemical Name:3-IODO-5,7-DIMETHYL (1H)INDAZOLE
CAS No.:847906-31-4
Molecular Formula:C₉H₉IN₂
Molecular Weight:272.088
Hs Code.:
Mol file:847906-31-4.mol

Synonyms:3-IODO-5,7-DIMETHYL (1H)INDAZOLE

Suppliers and Price of 3-IODO-5,7-DIMETHYL (1H)INDAZOLE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Iodo-5,7-dimethyl(1H)indazole
50mg
$ 45.00

Crysdot
3-Iodo-5,7-dimethyl-1H-indazole 97%
5g
$ 774.00

Crysdot
3-Iodo-5,7-dimethyl-1H-indazole 97%
1g
$ 359.00

Crysdot
3-Iodo-5,7-dimethyl-1H-indazole 97%
10g
$ 1037.00

Crysdot
3-Iodo-5,7-dimethyl-1H-indazole 97%
25g
$ 1870.00

Chemenu
3-Iodo-5,7-dimethyl-1H-indazole 97%
25g
$ 1762.00

Chemenu
3-Iodo-5,7-dimethyl-1H-indazole 97%
10g
$ 977.00

Chemenu
3-Iodo-5,7-dimethyl-1H-indazole 97%
1g
$ 339.00

Chemenu
3-Iodo-5,7-dimethyl-1H-indazole 97%
5g
$ 731.00

American Custom Chemicals Corporation
3-IODO-5,7-DIMETHYL (1H)INDAZOLE 95.00%
100MG
$ 467.25

Total 6 raw suppliers

Chemical Property of 3-IODO-5,7-DIMETHYL (1H)INDAZOLE

Chemical Property:

PSA：28.68000
LogP:2.78430

Purity/Quality:

97% ^*data from raw suppliers

3-Iodo-5,7-dimethyl(1H)indazole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-IODO-5,7-DIMETHYL (1H)INDAZOLE

There total 1 articles about 3-IODO-5,7-DIMETHYL (1H)INDAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 43067-41-0
6,7-dimethyl benzo(1,2-c)imidazole

: 847906-31-4
3-iodo-5,7-dimethyl-1H-indazole

Guidance literature:: With potassium hydroxide; iodine; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 2h;

Reference yield:

: 847906-31-4
3-iodo-5,7-dimethyl-1H-indazole

: 2,2-dimethylpropionic acid (R)-4-{4-[4-(5,7-dimethylindazol-2-yl)piperidine-1-carbonyl]phenyl}-4-methyl-2,5-dioxoimidazolidin-1-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: diethylazodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 3.5 h / 20 °C / Cooling with ice

2: hydrogen; palladium 10% on activated carbon; sodium hydroxide / water; tetrahydrofuran; methanol / 20 °C

3: hydrogenchloride / water; 1,4-dioxane / 20 °C

4: 1-hydroxy-7-aza-benzotriazole; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; sodium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; toluene;

Reference yield:

: 847906-31-4
3-iodo-5,7-dimethyl-1H-indazole

: (R)-5-{4-[4-(5,7-dimethylindazol-2-yl)piperidine-1-carbonyl]phenyl}-5-isopropylimidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: diethylazodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 3.5 h / 20 °C / Cooling with ice

2: hydrogen; palladium 10% on activated carbon; sodium hydroxide / water; tetrahydrofuran; methanol / 20 °C

3: hydrogenchloride / water; 1,4-dioxane / 20 °C

4: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / chloroform / 3.5 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; sodium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; methanol; chloroform; water; toluene;