Technology Process of C24H29N7O2
There total 9 articles about C24H29N7O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutylammomium bromide; potassium hydroxide;
In
2-methyltetrahydrofuran; water;
at 50 ℃;
for 23h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / 1,2-dimethoxyethane; water / 100 °C / Inert atmosphere
2: N,N-dimethyl-formamide; trichlorophosphate / 1,2-dichloro-ethane / 3 h / 80 °C
3: propan-1-ol / 4 h / 100 °C
4: tetrabutylammomium bromide; potassium hydroxide / 2-methyltetrahydrofuran; water / 23 h / 50 °C
With
tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide; sodium carbonate; N,N-dimethyl-formamide; potassium hydroxide; trichlorophosphate;
In
2-methyltetrahydrofuran; propan-1-ol; 1,2-dimethoxyethane; water; 1,2-dichloro-ethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogen bromide; acetic acid / 3 h / 40 - 50 °C
2: N,N-dimethyl-formamide; trichlorophosphate / 1,2-dichloro-ethane / 3 h / 80 °C
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / 1,2-dimethoxyethane; water / 2 h / Inert atmosphere; Reflux
4: propan-1-ol / 4 h / 100 °C
5: tetrabutylammomium bromide; potassium hydroxide / 2-methyltetrahydrofuran; water / 23 h / 50 °C
With
tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide; hydrogen bromide; sodium carbonate; acetic acid; N,N-dimethyl-formamide; potassium hydroxide; trichlorophosphate;
In
2-methyltetrahydrofuran; propan-1-ol; 1,2-dimethoxyethane; water; 1,2-dichloro-ethane;