iso-butyl 3-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

Base Information

Chemical Name:iso-butyl 3-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate
CAS No.:1252813-53-8
Molecular Formula:C₁₉H₂₉BO₄
Molecular Weight:332.248
Hs Code.:

Synonyms:iso-butyl 3-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

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Chemical Property of iso-butyl 3-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

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Technology Process of iso-butyl 3-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

There total 2 articles about iso-butyl 3-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122-67-8
2-propenoic acid, 3-phenyl-, 2-methylpropyl ester

: 73183-34-3
bis(pinacol)diborane

: iso-butyl 3-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

: 1252813-53-8
iso-butyl 3-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

Guidance literature:: With methanol; ((2S,3S)-6-mesityl-2,3-diphenyl-2,3,5,6-tetrahydroimidazo[1,2-c]quinazolin-5-yl)copper(I) chloride; sodium t-butanolate; In toluene; at -55 ℃; for 6h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ol1021756

Reference yield:

: 122-67-8
2-propenoic acid, 3-phenyl-, 2-methylpropyl ester

: 73183-34-3
bis(pinacol)diborane

: 1252813-53-8
iso-butyl 3-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

Guidance literature:: bis(pinacol)diborane; With copper(I) oxide; C₃₁H₃₄N₃O⁽¹⁺⁾*Cl^(1-); caesium carbonate; In 1,2-dimethoxyethane; at 20 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;

2-propenoic acid, 3-phenyl-, 2-methylpropyl ester; In methanol; 1,2-dimethoxyethane; at 0 ℃; for 4h; enantioselective reaction;
DOI:10.1021/jo5021135