octyl 6-O-acetyl-2,3-di-O-benzyl-4-O-phenoxythiocarbonyl-β-D-glucopyranoside

Base Information

Chemical Name:octyl 6-O-acetyl-2,3-di-O-benzyl-4-O-phenoxythiocarbonyl-β-D-glucopyranoside
CAS No.:118249-77-7
Molecular Formula:C₃₇H₄₆O₈S
Molecular Weight:650.833
Hs Code.:

Synonyms:octyl 6-O-acetyl-2,3-di-O-benzyl-4-O-phenoxythiocarbonyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of octyl 6-O-acetyl-2,3-di-O-benzyl-4-O-phenoxythiocarbonyl-β-D-glucopyranoside

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Technology Process of octyl 6-O-acetyl-2,3-di-O-benzyl-4-O-phenoxythiocarbonyl-β-D-glucopyranoside

There total 6 articles about octyl 6-O-acetyl-2,3-di-O-benzyl-4-O-phenoxythiocarbonyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 118249-76-6
octyl 6-O-acetyl-2,3-di-O-benzyl-β-D-glucopyranoside

: 1005-56-7
phenylcarbonochloridothioate

: 118249-77-7
octyl 6-O-acetyl-2,3-di-O-benzyl-4-O-phenoxythiocarbonyl-β-D-glucopyranoside

Guidance literature:: With dmap; In acetonitrile; for 5h; Heating;
DOI:10.1016/0008-6215(88)84115-6

Reference yield:

: 100-39-0
benzyl bromide

: 118249-77-7
octyl 6-O-acetyl-2,3-di-O-benzyl-4-O-phenoxythiocarbonyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: NaH (60percent, dispersion im oil) / dimethylformamide / 20 h / Ambient temperature

2: 86 percent / aq. 80percent acetic acid / CH₂Cl₂ / 2 h / 80 °C

3: 71.6 percent / pyridine / CH₂Cl₂ / 1) -78 deg C, 3 h: 2) 0 deg C, 1 h

4: 52 percent / 4-dimethylaminopyridine / acetonitrile / 5 h / Heating

With pyridine; dmap; sodium hydride; acetic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0008-6215(88)84115-6

Reference yield:

: 118249-73-3
n-octyl 4,6-O-benzylidene-β-D-glucopyranoside

: 118249-77-7
octyl 6-O-acetyl-2,3-di-O-benzyl-4-O-phenoxythiocarbonyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: NaH (60percent, dispersion im oil) / dimethylformamide / 20 h / Ambient temperature

2: 86 percent / aq. 80percent acetic acid / CH₂Cl₂ / 2 h / 80 °C

3: 71.6 percent / pyridine / CH₂Cl₂ / 1) -78 deg C, 3 h: 2) 0 deg C, 1 h

4: 52 percent / 4-dimethylaminopyridine / acetonitrile / 5 h / Heating

With pyridine; dmap; sodium hydride; acetic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0008-6215(88)84115-6