methyl 2,3-di-O-benzyl-7,8,9-trideoxy-4-O-(4-methoxybenzyl)-L-glycero-α-D-gluco-non-8-enopyranoside

Base Information

Chemical Name:methyl 2,3-di-O-benzyl-7,8,9-trideoxy-4-O-(4-methoxybenzyl)-L-glycero-α-D-gluco-non-8-enopyranoside
CAS No.:130524-00-4
Molecular Formula:C₃₂H₃₈O₇
Molecular Weight:534.65
Hs Code.:

Synonyms:methyl 2,3-di-O-benzyl-7,8,9-trideoxy-4-O-(4-methoxybenzyl)-L-glycero-α-D-gluco-non-8-enopyranoside

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Chemical Property of methyl 2,3-di-O-benzyl-7,8,9-trideoxy-4-O-(4-methoxybenzyl)-L-glycero-α-D-gluco-non-8-enopyranoside

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of methyl 2,3-di-O-benzyl-7,8,9-trideoxy-4-O-(4-methoxybenzyl)-L-glycero-α-D-gluco-non-8-enopyranoside

There total 1 articles about methyl 2,3-di-O-benzyl-7,8,9-trideoxy-4-O-(4-methoxybenzyl)-L-glycero-α-D-gluco-non-8-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130523-98-7
(2S,3S,4S,5R,6S)-4,5-Bis-benzyloxy-6-methoxy-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-carbaldehyde

: 1730-25-2
allylmagnesium bromide

: 130523-99-8
methyl 2,3-di-O-benzyl-7,8,9-trideoxy-4-O-(4-methoxybenzyl)-D-glycero-α-D-gluco-non-8-enopyranoside

: 130524-00-4
methyl 2,3-di-O-benzyl-7,8,9-trideoxy-4-O-(4-methoxybenzyl)-L-glycero-α-D-gluco-non-8-enopyranoside

Guidance literature:: In tetrahydrofuran; for 0.25h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

Reference yield:

: 130524-00-4
methyl 2,3-di-O-benzyl-7,8,9-trideoxy-4-O-(4-methoxybenzyl)-L-glycero-α-D-gluco-non-8-enopyranoside

: 130524-01-5
methyl 2,3-di-O-benzyl-7-deoxy-4-O-(4-methoxybenzyl)-L-glycero-α-D-gluco-octopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) ozone, 2.) dimethyl sulfide / 1.) methanol, dichloromethane, -78 deg C, 20 min, 2.) RT, 30 min

2: sodium borohydride / methanol; CH₂Cl₂ / 0.5 h / Ambient temperature

With sodium tetrahydroborate; dimethylsulfide; ozone; In methanol; dichloromethane;

Reference yield:

: 130524-00-4
methyl 2,3-di-O-benzyl-7,8,9-trideoxy-4-O-(4-methoxybenzyl)-L-glycero-α-D-gluco-non-8-enopyranoside

: 130524-03-7
methyl 4,6,8-tri-O-acetyl-2,3-di-O-benzyl-7-deoxy-L-glycero-α-D-gluco-octopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) ozone, 2.) dimethyl sulfide / 1.) methanol, dichloromethane, -78 deg C, 20 min, 2.) RT, 30 min

2: sodium borohydride / methanol; CH₂Cl₂ / 0.5 h / Ambient temperature

3: 80 percent / ceric ammonium nitrate / acetonitrile; H₂O / 0.75 h / Ambient temperature

4: 99 percent / N,N-(dimethylamino)pyridine, pyridine / 2 h / Ambient temperature

With pyridine; dmap; sodium tetrahydroborate; ammonium cerium(IV) nitrate; dimethylsulfide; ozone; In methanol; dichloromethane; water; acetonitrile;