6-(4-chlorophenylsulfonyl)-N-(2,4-dichlorobenzyl)-1,6-diazaspiro[3.3]heptane-1-carboxamide

Base Information

Chemical Name:6-(4-chlorophenylsulfonyl)-N-(2,4-dichlorobenzyl)-1,6-diazaspiro[3.3]heptane-1-carboxamide
CAS No.:1431868-40-4
Molecular Formula:C₁₉H₁₈Cl₃N₃O₃S
Molecular Weight:474.795
Hs Code.:

Synonyms:6-(4-chlorophenylsulfonyl)-N-(2,4-dichlorobenzyl)-1,6-diazaspiro[3.3]heptane-1-carboxamide

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Chemical Property of 6-(4-chlorophenylsulfonyl)-N-(2,4-dichlorobenzyl)-1,6-diazaspiro[3.3]heptane-1-carboxamide

Chemical Property:

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Technology Process of 6-(4-chlorophenylsulfonyl)-N-(2,4-dichlorobenzyl)-1,6-diazaspiro[3.3]heptane-1-carboxamide

There total 7 articles about 6-(4-chlorophenylsulfonyl)-N-(2,4-dichlorobenzyl)-1,6-diazaspiro[3.3]heptane-1-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1431868-64-2
N-(2,4-dichlorobenzyl)-1,6-diazaspiro[3.3]heptane-1-carboxamide

: 98-60-2
4-chlorobenzenesulfonyl chloride

: 1431868-40-4
6-(4-chlorophenylsulfonyl)-N-(2,4-dichlorobenzyl)-1,6-diazaspiro[3.3]heptane-1-carboxamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 1431868-59-5
tert-butyl 1-benzyl-1,6-diazaspiro[3.3]heptane-6-carboxylate

: 1431868-40-4
6-(4-chlorophenylsulfonyl)-N-(2,4-dichlorobenzyl)-1,6-diazaspiro[3.3]heptane-1-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 48 h / 20 °C

2: triethylamine / acetonitrile / 20 °C

3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

4: triethylamine / dichloromethane / 20 °C

With palladium 10% on activated carbon; hydrogen; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; acetonitrile;

Reference yield:

: 1431868-63-1
tert-butyl 1-(2,4-dichlorobenzylcarbamoyl)-1,6-diazaspiro[3.3]heptane-6-carboxylate

: 1431868-40-4
6-(4-chlorophenylsulfonyl)-N-(2,4-dichlorobenzyl)-1,6-diazaspiro[3.3]heptane-1-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

2: triethylamine / dichloromethane / 20 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;