Nicotinamide, 6-(methylsulfonyl)- (5CI)

Base Information

• Chemical Name: Nicotinamide, 6-(methylsulfonyl)- (5CI)
• CAS No.: 845875-80-1
• Molecular Formula: C₇H₈N₂O₃S
• Molecular Weight: 200.218
• Hs Code.: 2933399090
• Mol file: 845875-80-1.mol

Synonyms:Nicotinamide,6-(methylsulfonyl)- (5CI)

Chemical Property of Nicotinamide, 6-(methylsulfonyl)- (5CI)

Chemical Property:

• PSA: 98.50000
• LogP: 1.36510

Purity/Quality:

97% ^*data from raw suppliers

6-(Methylsulfonyl)nicotinamide 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Nicotinamide, 6-(methylsulfonyl)- (5CI)

There total 2 articles about Nicotinamide, 6-(methylsulfonyl)- (5CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methylthio-5-pyridinecarboxamide (7151-91-9) → 6-methanesulfonyl-nicotinic acid amide (845875-80-1)

Guidance literature:

With potassium permanganate; sulfuric acid; acetone;

DOI:10.1039/jr9480001939

Reference yield:

6-mercapto-nicotinamide (7151-89-5) → 6-methanesulfonyl-nicotinic acid amide (845875-80-1)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₃I; aq.-ethanolic NaOH

2: acetone; aqueous H₂SO₄; KMnO₄

With sodium hydroxide; potassium permanganate; sulfuric acid; acetone; methyl iodide;

DOI:10.1039/jr9480001939

Reference yield:

6-methanesulfonyl-nicotinic acid amide (845875-80-1) → 6-(methylsulfonyl)nicotinonitrile (66154-68-5)

Guidance literature:

With chloroform; trichlorophosphate;

DOI:10.1039/jr9480001939

upstream raw materials:

2-methylthio-5-pyridinecarboxamide

6-mercapto-nicotinamide

Downstream raw materials:

6-(methylsulfonyl)nicotinonitrile

6-methanesulfonyl-nicotinamidine

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