N-[3-cyano-3-ethoxy-5,6-dimethyl-1(3H)-isobenzofuranylidene]-2-methyl-2-propanamine

Base Information

Chemical Name:N-[3-cyano-3-ethoxy-5,6-dimethyl-1(3H)-isobenzofuranylidene]-2-methyl-2-propanamine
CAS No.:1449007-87-7
Molecular Formula:C₁₇H₂₂N₂O₂
Molecular Weight:286.374
Hs Code.:

Synonyms:N-[3-cyano-3-ethoxy-5,6-dimethyl-1(3H)-isobenzofuranylidene]-2-methyl-2-propanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[3-cyano-3-ethoxy-5,6-dimethyl-1(3H)-isobenzofuranylidene]-2-methyl-2-propanamine

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Technology Process of N-[3-cyano-3-ethoxy-5,6-dimethyl-1(3H)-isobenzofuranylidene]-2-methyl-2-propanamine

There total 1 articles about N-[3-cyano-3-ethoxy-5,6-dimethyl-1(3H)-isobenzofuranylidene]-2-methyl-2-propanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 623-49-4
ethyl cyanoformate

: 458566-99-9
4,5-dimethyl-2-(trimethylsilyl)phenyl triflate

: 1449007-87-7
N-[3-cyano-3-ethoxy-5,6-dimethyl-1(3H)-isobenzofuranylidene]-2-methyl-2-propanamine

: 1615677-54-7
(Z)-ethyl 2-[(tert-butylimino)(cyano)methyl]-4,5-dimethylbenzoate

Guidance literature:: With potassium fluoride; [Pd(PhCN)₂(dppf)](BF₄)₂; 18-crown-6 ether; In tetrahydrofuran; at 50 ℃; for 18h; Schlenk technique; Inert atmosphere;
DOI:10.1021/om500408h

Reference yield: 89.0%

: 1449007-87-7
N-[3-cyano-3-ethoxy-5,6-dimethyl-1(3H)-isobenzofuranylidene]-2-methyl-2-propanamine

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 4,5-dimethyl ethyl 2-cyanobenzoate

Guidance literature:: With tris(pentafluorophenyl)borate; In tetrahydrofuran; at 70 ℃; for 8h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol5026519