2-[2,5-dibromo-3-(1,1-dimethyl-2-oxo-ethyl)-phenyl]-2-methyl-propionaldehyde

Base Information

Chemical Name:2-[2,5-dibromo-3-(1,1-dimethyl-2-oxo-ethyl)-phenyl]-2-methyl-propionaldehyde
CAS No.:740815-84-3
Molecular Formula:C₁₄H₁₆Br₂O₂
Molecular Weight:376.088
Hs Code.:

Synonyms:2-[2,5-dibromo-3-(1,1-dimethyl-2-oxo-ethyl)-phenyl]-2-methyl-propionaldehyde

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Chemical Property of 2-[2,5-dibromo-3-(1,1-dimethyl-2-oxo-ethyl)-phenyl]-2-methyl-propionaldehyde

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Technology Process of 2-[2,5-dibromo-3-(1,1-dimethyl-2-oxo-ethyl)-phenyl]-2-methyl-propionaldehyde

There total 1 articles about 2-[2,5-dibromo-3-(1,1-dimethyl-2-oxo-ethyl)-phenyl]-2-methyl-propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 740815-83-2
2,5-dibromo-1,3-bis(1-cyano-1-methylethyl)benzene

: 740815-84-3
2-[2,5-dibromo-3-(1,1-dimethyl-2-oxo-ethyl)-phenyl]-2-methyl-propionaldehyde

Guidance literature:: With diisobutylaluminium hydride; In hexane; benzene; at 20 ℃; for 2h;
DOI:10.1021/jo049571q

Reference yield: 20.0%

: 740815-84-3
2-[2,5-dibromo-3-(1,1-dimethyl-2-oxo-ethyl)-phenyl]-2-methyl-propionaldehyde

: 740815-80-9
2,5-dibromo-1,3-di-tert-butylbenzene

Guidance literature:: With potassium hydroxide; hydrazine hydrate; In 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; at 130 - 200 ℃; for 7h;
DOI:10.1021/jo049571q

Reference yield:

: 740815-84-3
2-[2,5-dibromo-3-(1,1-dimethyl-2-oxo-ethyl)-phenyl]-2-methyl-propionaldehyde

: 19715-31-2
5-amino-2-bromo-1,3-di-tert-butylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 20 percent / hydrazine monohydrate; KOH / triethylene glycol / 7 h / 130 - 200 °C

2: 97 percent / DPPF; NaOt-Bu / Pd(OAc)2 / toluene / 10 h / 95 °C

3: 57 percent / hydrochloric acid / tetrahydrofuran / 1 h / Heating

With hydrogenchloride; 1,1'-bis-(diphenylphosphino)ferrocene; potassium hydroxide; hydrazine hydrate; sodium t-butanolate; palladium diacetate; In tetrahydrofuran; toluene; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; 1: Wolff-Kishner reduction (Huang-Minlon method);
DOI:10.1021/jo049571q