C₁₄H₁₁F₃O₂

Base Information

Chemical Name:C₁₄H₁₁F₃O₂
CAS No.:1440059-09-5
Molecular Formula:C₁₄H₁₁F₃O₂
Molecular Weight:268.235
Hs Code.:

C<sub>14</sub>H<sub>11</sub>F<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₄H₁₁F₃O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₁F₃O₂

Chemical Property:

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Technology Process of C₁₄H₁₁F₃O₂

There total 1 articles about C₁₄H₁₁F₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 474709-28-9
4,4,5,5-tetramethyl-2-(4-(trifluoromethyloxy)phenyl)-1,3,2-dioxaborolane

: 17933-03-8
m-tolylboronic acid

: 1440059-09-5
C₁₄H₁₁F₃O₂

Guidance literature:: 4,4,5,5-tetramethyl-2-(4-(trifluoromethyloxy)phenyl)-1,3,2-dioxaborolane; m-tolylboronic acid; With Oxone; potassium phosphate; In water; at 70 ℃;

With copper diacetate; triethylamine; In ethanol; water; acetonitrile; at 80 ℃; chemoselective reaction;
DOI:10.1039/C6SC04014D

Reference yield:

: 1440059-09-5
C₁₄H₁₁F₃O₂

: 4755-77-5
Ethyl oxalyl chloride

: 1440061-37-9
C₁₈H₁₅F₃O₅

Guidance literature:: With aluminum (III) chloride; In dichloromethane; at 5 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c3nj00032j

Reference yield:

: 1440059-09-5
C₁₄H₁₁F₃O₂

: 1440060-70-7
C₂₃H₁₆F₅NO₃

Guidance literature:: Multi-step reaction with 6 steps

1: aluminum (III) chloride / dichloromethane / 2 h / 5 - 20 °C / Inert atmosphere

2: hydroxylamine hydrochloride / ethanol / 5 h / Reflux; Inert atmosphere

3: sodium tetrahydroborate; iodine / tetrahydrofuran / 7.5 h / 0 °C / Reflux; Inert atmosphere

4: triethylamine / tetrahydrofuran / 2 h / 5 - 20 °C / Inert atmosphere

5: thionyl chloride / toluene / 3 h / 80 °C / Inert atmosphere

6: sodium hydroxide / methanol / 1 h / 50 °C / Inert atmosphere

With aluminum (III) chloride; sodium tetrahydroborate; thionyl chloride; hydroxylamine hydrochloride; iodine; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; toluene; 1: |Friedel-Crafts Acylation;
DOI:10.1039/c3nj00032j