(μ-dinitrogen)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

Base Information

Chemical Name:(μ-dinitrogen)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))
CAS No.:129873-48-9
Molecular Formula:C₁₀₂H₁₀₈N₁₄Ru₂
Molecular Weight:1732.21
Hs Code.:

Synonyms:(μ-dinitrogen)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (μ-dinitrogen)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

Chemical Property:

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Technology Process of (μ-dinitrogen)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

There total 8 articles about (μ-dinitrogen)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 132674-18-1
bis(ammine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 132674-20-5
(μ-diazene)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 129873-48-9
(μ-dinitrogen)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 132674-19-2
(μ-hydrazine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

Guidance literature:: With tert.-butylhydroperoxide; monitored by (1)H-NMR;
DOI:10.1021/ja00047a016

Reference yield: 9.0%

: ferrocenium hexafluorophosphate

: 132674-18-1
bis(ammine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 132674-20-5
(μ-diazene)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 129873-48-9
(μ-dinitrogen)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 132674-19-2
(μ-hydrazine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

Guidance literature:: With sodium methylate; In benzene; monitored by (1)H-NMR;
DOI:10.1021/ja00047a016

Reference yield:

: 106935-77-7
C₇₆H₇₆N₈Ru₂

: 71333-67-0
1-t-butyl-5-phenylimidazole

: 129873-48-9
(μ-dinitrogen)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

Guidance literature:: With nitrogen; In benzene; Under N2 a soln. of 1-tert.-butyl-5-phenylimidazole in benzene is added to a soln. of Ru2DPB in dry deaerated benzene.; After 30 min stirring the solvent is removed under reduced pressure to yield Ru2(N2) quantitatively.;