(μ-hydrazine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

Base Information

Chemical Name:(μ-hydrazine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))
CAS No.:132674-19-2
Molecular Formula:C₁₀₂H₁₁₂N₁₄Ru₂
Molecular Weight:1736.25
Hs Code.:

Synonyms:(μ-hydrazine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

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Chemical Property of (μ-hydrazine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

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Technology Process of (μ-hydrazine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

There total 4 articles about (μ-hydrazine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 132674-18-1
bis(ammine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 132674-20-5
(μ-diazene)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 129873-48-9
(μ-dinitrogen)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 132674-19-2
(μ-hydrazine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

Guidance literature:: With tert.-butylhydroperoxide; monitored by (1)H-NMR;
DOI:10.1021/ja00047a016

Reference yield: 9.0%

: ferrocenium hexafluorophosphate

: 132674-18-1
bis(ammine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 132674-20-5
(μ-diazene)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 129873-48-9
(μ-dinitrogen)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 132674-19-2
(μ-hydrazine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

Guidance literature:: With sodium methylate; In benzene; monitored by (1)H-NMR;
DOI:10.1021/ja00047a016

Reference yield:

: 129873-48-9
(μ-dinitrogen)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

: 132674-19-2
(μ-hydrazine)diruthenium(II)DPB(bis-(1-tert-butyl-5-phenylimidazole))

Guidance literature:: With nitrogen; hydrazine; In toluene; A soln. of Ru2(N2) in toluene is stirred with anhydrous N2H4 under an N2 atmos. for 24 h.; After removal of the solvent under reduced pressure the hydrazine complex Ru2(N2H4) is obtd. in quantitative yield.;