Methyl <(R)-2-methanesulfonyloxy-3-(4-methoxy-benzyloxy)-propyl> malonate

Base Information

Chemical Name:Methyl <(R)-2-methanesulfonyloxy-3-(4-methoxy-benzyloxy)-propyl> malonate
CAS No.:131072-38-3
Molecular Formula:C₁₆H₂₂O₉S
Molecular Weight:390.411
Hs Code.:

Synonyms:Methyl <(R)-2-methanesulfonyloxy-3-(4-methoxy-benzyloxy)-propyl> malonate

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Chemical Property of Methyl <(R)-2-methanesulfonyloxy-3-(4-methoxy-benzyloxy)-propyl> malonate

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Technology Process of Methyl <(R)-2-methanesulfonyloxy-3-(4-methoxy-benzyloxy)-propyl> malonate

There total 3 articles about Methyl <(R)-2-methanesulfonyloxy-3-(4-methoxy-benzyloxy)-propyl> malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 131072-37-2
Methyl <(R)-2-hydroxy-3-(4-methoxy-benzyloxy)-propyl> malonate

: 124-63-0
methanesulfonyl chloride

: 131072-38-3
Methyl <(R)-2-methanesulfonyloxy-3-(4-methoxy-benzyloxy)-propyl> malonate

Guidance literature:: With triethylamine; In dichloromethane; at 40 ℃; for 2h;
DOI:10.1016/S0040-4020(01)87922-9

Reference yield:

: 131072-36-1
Methyl <(R)-2-allyloxy-3-(4-methoxy-benzyloxy)-propyl> malonate

: 131072-38-3
Methyl <(R)-2-methanesulfonyloxy-3-(4-methoxy-benzyloxy)-propyl> malonate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / PdCl₂ / acetic acid; H₂O / 19.5 h / 20 °C

2: 81 percent / NEt₃ / CH₂Cl₂ / 2 h / 40 °C

With triethylamine; palladium dichloride; In dichloromethane; water; acetic acid;
DOI:10.1016/S0040-4020(01)87922-9

Reference yield:

: 114935-26-1
(R)-2-Allyloxy-3-(4-methoxy-benzyloxy)-propan-1-ol

: 131072-38-3
Methyl <(R)-2-methanesulfonyloxy-3-(4-methoxy-benzyloxy)-propyl> malonate

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / NEt₃ / CH₂Cl₂ / 0.25 h / 20 °C

2: 90 percent / PdCl₂ / acetic acid; H₂O / 19.5 h / 20 °C

3: 81 percent / NEt₃ / CH₂Cl₂ / 2 h / 40 °C

With triethylamine; palladium dichloride; In dichloromethane; water; acetic acid;
DOI:10.1016/S0040-4020(01)87922-9