(S)-2-amino-3-(4-(2-(hydroxyamino)-2-oxoethoxy)phenyl)-N-phenylpropanamide hydrochloride

Base Information

Chemical Name:(S)-2-amino-3-(4-(2-(hydroxyamino)-2-oxoethoxy)phenyl)-N-phenylpropanamide hydrochloride
CAS No.:1323433-87-9
Molecular Formula:C₁₇H₁₉N₃O₄*ClH
Molecular Weight:365.817
Hs Code.:

Synonyms:(S)-2-amino-3-(4-(2-(hydroxyamino)-2-oxoethoxy)phenyl)-N-phenylpropanamide hydrochloride

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Chemical Property of (S)-2-amino-3-(4-(2-(hydroxyamino)-2-oxoethoxy)phenyl)-N-phenylpropanamide hydrochloride

Chemical Property:

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Technology Process of (S)-2-amino-3-(4-(2-(hydroxyamino)-2-oxoethoxy)phenyl)-N-phenylpropanamide hydrochloride

There total 5 articles about (S)-2-amino-3-(4-(2-(hydroxyamino)-2-oxoethoxy)phenyl)-N-phenylpropanamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1323433-86-8
(S)-tert-butyl (3-(4-(2-(hydroxyamino)-2-oxoethoxy)phenyl)-1-oxo-1-(phenylamino)propan-2-yl)carbamate

: 1323433-87-9
(S)-2-amino-3-(4-(2-(hydroxyamino)-2-oxoethoxy)phenyl)-N-phenylpropanamide hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 20 ℃; for 7h;
DOI:10.1016/j.bmc.2011.06.046

Reference yield:

: 179631-88-0
(S)-tert-butyl (3-(4-hydroxyphenyl)-1-oxo-1-(phenylamino)propan-2-yl)carbamate

: 1323433-87-9
(S)-2-amino-3-(4-(2-(hydroxyamino)-2-oxoethoxy)phenyl)-N-phenylpropanamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

2.1: hydroxylamine potassium salt / methanol / 0.5 h

2.2: pH 3 - 4

3.1: hydrogenchloride / ethyl acetate / 7 h / 20 °C

With hydrogenchloride; hydroxylamine potassium salt; potassium carbonate; In methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.06.046

Reference yield:

: 1323434-06-5
(S)-methyl 2-(4-(2-((tert-butoxycarbonyl)amino)-3-oxo-3-(phenylamino)propyl)phenoxy)acetate

: 1323433-87-9
(S)-2-amino-3-(4-(2-(hydroxyamino)-2-oxoethoxy)phenyl)-N-phenylpropanamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine potassium salt / methanol / 0.5 h

1.2: pH 3 - 4

2.1: hydrogenchloride / ethyl acetate / 7 h / 20 °C

With hydrogenchloride; hydroxylamine potassium salt; In methanol; ethyl acetate;
DOI:10.1016/j.bmc.2011.06.046