(S)-tert-butyl (3-(4-hydroxyphenyl)-1-oxo-1-(phenylamino)propan-2-yl)carbamate

Base Information

Chemical Name:(S)-tert-butyl (3-(4-hydroxyphenyl)-1-oxo-1-(phenylamino)propan-2-yl)carbamate
CAS No.:179631-88-0
Molecular Formula:C₂₀H₂₄N₂O₄
Molecular Weight:356.422
Hs Code.:

Synonyms:(S)-tert-butyl (3-(4-hydroxyphenyl)-1-oxo-1-(phenylamino)propan-2-yl)carbamate

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Chemical Property of (S)-tert-butyl (3-(4-hydroxyphenyl)-1-oxo-1-(phenylamino)propan-2-yl)carbamate

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Technology Process of (S)-tert-butyl (3-(4-hydroxyphenyl)-1-oxo-1-(phenylamino)propan-2-yl)carbamate

There total 5 articles about (S)-tert-butyl (3-(4-hydroxyphenyl)-1-oxo-1-(phenylamino)propan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 3978-80-1
Boc-Tyr-OH

: N-tert-butyl-N'-phenyl-S-phenylisothiourea

: 179631-88-0
(S)-tert-butyl (3-(4-hydroxyphenyl)-1-oxo-1-(phenylamino)propan-2-yl)carbamate

Guidance literature:: With iron(III)-acetylacetonate; In isopropyl alcohol; at 83 ℃; for 72h; regioselective reaction; Sealed tube;
DOI:10.1002/adsc.201700134

Reference yield: 29.0%

: 3978-80-1
Boc-Tyr-OH

: 62-53-3
aniline

: 179631-88-0
(S)-tert-butyl (3-(4-hydroxyphenyl)-1-oxo-1-(phenylamino)propan-2-yl)carbamate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1246/cl.2008.1028

Reference yield:

: 3978-80-1
Boc-Tyr-OH

: 62-53-3
aniline

: tert-butyl-(3-(4-hydroxyphenyl)-1-oxo-1-(phenylamino)propan-2-yl)carbamate

: 179631-88-0
(S)-tert-butyl (3-(4-hydroxyphenyl)-1-oxo-1-(phenylamino)propan-2-yl)carbamate

Guidance literature:: With fluorosulfonyl fluoride; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 5h; Overall yield = 99 %; Overall yield = 352.9 mg;
DOI:10.1039/c9ob00699k