2-((1R,4S,5R,6R)-4,5,6-Tris-benzyloxy-cyclohex-2-enyl)-isoindole-1,3-dione

Base Information

Chemical Name:2-((1R,4S,5R,6R)-4,5,6-Tris-benzyloxy-cyclohex-2-enyl)-isoindole-1,3-dione
CAS No.:157494-41-2
Molecular Formula:C₃₅H₃₁NO₅
Molecular Weight:545.635
Hs Code.:

Synonyms:2-((1R,4S,5R,6R)-4,5,6-Tris-benzyloxy-cyclohex-2-enyl)-isoindole-1,3-dione

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Chemical Property of 2-((1R,4S,5R,6R)-4,5,6-Tris-benzyloxy-cyclohex-2-enyl)-isoindole-1,3-dione

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Technology Process of 2-((1R,4S,5R,6R)-4,5,6-Tris-benzyloxy-cyclohex-2-enyl)-isoindole-1,3-dione

There total 1 articles about 2-((1R,4S,5R,6R)-4,5,6-Tris-benzyloxy-cyclohex-2-enyl)-isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 136918-14-4,85-41-6
phthalimide

: 102997-58-0
(1R,2R,3S)-tris(phenylmethoxy)-6S-hydroxy-cyclohex-4-ene

: 157494-41-2
2-((1R,4S,5R,6R)-4,5,6-Tris-benzyloxy-cyclohex-2-enyl)-isoindole-1,3-dione

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 3h; Ambient temperature;
DOI:10.1016/S0040-4039(00)76990-5

Reference yield: 100.0%

: 157494-41-2
2-((1R,4S,5R,6R)-4,5,6-Tris-benzyloxy-cyclohex-2-enyl)-isoindole-1,3-dione

: 157494-42-3
(1R,4S,5R,6R)-4,5,6-Tris-benzyloxy-cyclohex-2-enylamine

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Heating;
DOI:10.1016/S0040-4039(00)76990-5

Reference yield:

: 157494-41-2
2-((1R,4S,5R,6R)-4,5,6-Tris-benzyloxy-cyclohex-2-enyl)-isoindole-1,3-dione

: 157494-44-5
(2S,3R,4S,5R)-2,3,4-Tris-benzyloxy-5-tert-butoxycarbonylamino-hexanedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / hydrazine hydrate / ethanol / 2 h / Heating

2: 100 percent / CH₂Cl₂ / 4 h / Ambient temperature

3: 71 percent / O₃, 2.5M NaOH / CH₂Cl₂ / 4 h / -78 °C

With sodium hydroxide; ozone; hydrazine hydrate; In ethanol; dichloromethane;
DOI:10.1016/S0040-4039(00)76990-5