2-(p-tolylsulfonyl)ethanal ethylene ketal

Base Information

Chemical Name:2-(p-tolylsulfonyl)ethanal ethylene ketal
CAS No.:86410-03-9
Molecular Formula:C₁₁H₁₄O₄S
Molecular Weight:242.296
Hs Code.:

Synonyms:2-(p-tolylsulfonyl)ethanal ethylene ketal

Suppliers and Price of 2-(p-tolylsulfonyl)ethanal ethylene ketal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(p-tolylsulfonyl)ethanal ethylene ketal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(p-tolylsulfonyl)ethanal ethylene ketal

There total 3 articles about 2-(p-tolylsulfonyl)ethanal ethylene ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 86409-95-2
(E)-1-(phenylseleno)-2-(p-tolylsulfonyl)ethene Se-oxide

: 107-21-1
ethylene glycol

: 86410-03-9
2-(p-tolylsulfonyl)ethanal ethylene ketal

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; water; for 24h; Ambient temperature;
DOI:10.1021/jo00166a030

Reference yield:

: 68819-94-3
p-tolyl benzeneselenosulfonate

: 86410-03-9
2-(p-tolylsulfonyl)ethanal ethylene ketal

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / azobis(isobutyronitrile) / CH₂Cl₂ / 72 h / 80 °C / 646.4 Torr / Parr high-pressure reaction vessel

2: 97 percent / m-chloroperbenzoic acid / CH₂Cl₂; hexane / 0.17 h / Ambient temperature

3: 74 percent / KOH / tetrahydrofuran; H₂O / 24 h / Ambient temperature

With potassium hydroxide; 2,2'-azobis(isobutyronitrile); 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane; water;
DOI:10.1021/jo00166a030

Reference yield:

: 86409-89-4
(E)-1-(phenylseleno)-2-(p-tolylsulfonyl)ethene

: 86410-03-9
2-(p-tolylsulfonyl)ethanal ethylene ketal

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / m-chloroperbenzoic acid / CH₂Cl₂; hexane / 0.17 h / Ambient temperature

2: 74 percent / KOH / tetrahydrofuran; H₂O / 24 h / Ambient temperature

With potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane; water;
DOI:10.1021/jo00166a030