4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 4-formylphenylcarbamate

Base Information

Chemical Name:4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 4-formylphenylcarbamate
CAS No.:1349832-91-2
Molecular Formula:C₂₁H₂₄BNO₅
Molecular Weight:381.236
Hs Code.:

Synonyms:4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 4-formylphenylcarbamate

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Chemical Property of 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 4-formylphenylcarbamate

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Technology Process of 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 4-formylphenylcarbamate

There total 2 articles about 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 4-formylphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 619-66-9
4-Carboxybenzaldehyde

: 302348-51-2
(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

: 1349832-91-2
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 4-formylphenylcarbamate

Guidance literature:: With diphenylphosphoranyl azide; triethylamine; In 1,4-dioxane; at 105 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo2018763

Reference yield:

: 1349832-93-4
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 4-(dimethoxymethyl)phenylcarbamate

: 1349832-91-2
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 4-formylphenylcarbamate

Guidance literature:: In water-d2; [D₃]acetonitrile; at 25 ℃; for 6h; pH=10; aq. buffer;
DOI:10.1021/jo2018763

Reference yield: 95.0%

: 1825-61-2
Trimethylmethoxysilane

: 1349832-91-2
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 4-formylphenylcarbamate

: 1349832-93-4
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 4-(dimethoxymethyl)phenylcarbamate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - 25 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1021/jo2018763