Technology Process of C27H34BNO7S
There total 10 articles about C27H34BNO7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium acetate;
bis-triphenylphosphine-palladium(II) chloride;
In
1,4-dioxane;
for 2h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: copper(l) iodide / bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine / N,N-dimethyl-formamide / Inert atmosphere
1.2: 6 h / 75 °C / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / -30 - 20 °C
3.1: copper(l) iodide; triethylamine / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 2 h / 70 °C
4.1: gold(III) chloride / trifluoroacetic acid / 0.75 h / 100 °C / Sealed tube; Microwave Irradiation
5.1: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 2 h / Reflux
With
copper(l) iodide; tetrabutyl ammonium fluoride; potassium acetate; triethylamine;
gold(III) chloride; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide; trifluoroacetic acid;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / acetone / 20 °C
2: copper(l) iodide; triethylamine / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 2 h / 70 °C
3: gold(III) chloride / trifluoroacetic acid / 0.75 h / 100 °C / Sealed tube; Microwave Irradiation
4: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 2 h / Reflux
With
copper(l) iodide; potassium acetate; potassium carbonate; triethylamine;
gold(III) chloride; bis-triphenylphosphine-palladium(II) chloride;
In
1,4-dioxane; N,N-dimethyl-formamide; acetone; trifluoroacetic acid;