C₆₀H₇₈O₇

Base Information

Chemical Name:C₆₀H₇₈O₇
CAS No.:1558035-05-4
Molecular Formula:C₆₀H₇₈O₇
Molecular Weight:911.275
Hs Code.:

C<sub>60</sub>H<sub>78</sub>O<sub>7</sub>

Synonyms:C₆₀H₇₈O₇

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Chemical Property of C₆₀H₇₈O₇

Chemical Property:

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Technology Process of C₆₀H₇₈O₇

There total 9 articles about C₆₀H₇₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1558034-97-1
(3S,4R)-3-(benzyloxy)octadec-1-en-4-ol

: 82659-55-0
3-(2',3',4',6'-tetra-O-benzyl-α-D-galactopyranosyl)prop-1-ene

: 1558035-05-4
C₆₀H₇₈O₇

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 40 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol5002686

Reference yield:

: C₂₀H₃₈O₃

: 1558035-05-4
C₆₀H₇₈O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 12 h / 20 °C

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate; N-chloro-succinimide / dichloromethane; water / 12 h / 20 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 2 h / 0 - 20 °C / Inert atmosphere

4.1: acetyl chloride / methanol / 0.5 h / Inert atmosphere

5.1: toluene-4-sulfonic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / dichloromethane; hexane / 3.5 h / -78 - 20 °C / Inert atmosphere

7.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C / Inert atmosphere

7.2: 3 h / 0 - 20 °C / Inert atmosphere

8.1: sodium hydrogencarbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 0.42 h / 20 °C / Inert atmosphere

9.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 16 h / 40 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium 10% on activated carbon; potassium tert-butylate; tetrabutyl-ammonium chloride; hydrogen; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; acetyl chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol5002686

Reference yield:

: (2S,3R)-2,3-(O-isopropylidene)heptadecane-1,2,3-triol

: 1558035-05-4
C₆₀H₇₈O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate; N-chloro-succinimide / dichloromethane; water / 12 h / 20 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 2 h / 0 - 20 °C / Inert atmosphere

3.1: acetyl chloride / methanol / 0.5 h / Inert atmosphere

4.1: toluene-4-sulfonic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / dichloromethane; hexane / 3.5 h / -78 - 20 °C / Inert atmosphere

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C / Inert atmosphere

6.2: 3 h / 0 - 20 °C / Inert atmosphere

7.1: sodium hydrogencarbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 0.42 h / 20 °C / Inert atmosphere

8.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 16 h / 40 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium tert-butylate; tetrabutyl-ammonium chloride; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; acetyl chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol5002686