benzyl (6R,11R)-6-((2-(benzyloxy)-2-oxoethyl)carbamoyl)-11-((tert-butoxycarbonyl)amino)-2,2-dimethyl-4,12-dioxo-3-oxa-8,9-dithia-5,13-diazapentadecan-15-oate

Base Information

Chemical Name:benzyl (6R,11R)-6-((2-(benzyloxy)-2-oxoethyl)carbamoyl)-11-((tert-butoxycarbonyl)amino)-2,2-dimethyl-4,12-dioxo-3-oxa-8,9-dithia-5,13-diazapentadecan-15-oate
CAS No.:32381-30-9
Molecular Formula:C₃₄H₄₆N₄O₁₀S₂
Molecular Weight:734.892
Hs Code.:

benzyl (6R,11R)-6-((2-(benzyloxy)-2-oxoethyl)carbamoyl)-11-((tert-butoxycarbonyl)amino)-2,2-dimethyl-4,12-dioxo-3-oxa-8,9-dithia-5,13-diazapentadecan-15-oate

Synonyms:benzyl (6R,11R)-6-((2-(benzyloxy)-2-oxoethyl)carbamoyl)-11-((tert-butoxycarbonyl)amino)-2,2-dimethyl-4,12-dioxo-3-oxa-8,9-dithia-5,13-diazapentadecan-15-oate

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Chemical Property of benzyl (6R,11R)-6-((2-(benzyloxy)-2-oxoethyl)carbamoyl)-11-((tert-butoxycarbonyl)amino)-2,2-dimethyl-4,12-dioxo-3-oxa-8,9-dithia-5,13-diazapentadecan-15-oate

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Technology Process of benzyl (6R,11R)-6-((2-(benzyloxy)-2-oxoethyl)carbamoyl)-11-((tert-butoxycarbonyl)amino)-2,2-dimethyl-4,12-dioxo-3-oxa-8,9-dithia-5,13-diazapentadecan-15-oate

There total 2 articles about benzyl (6R,11R)-6-((2-(benzyloxy)-2-oxoethyl)carbamoyl)-11-((tert-butoxycarbonyl)amino)-2,2-dimethyl-4,12-dioxo-3-oxa-8,9-dithia-5,13-diazapentadecan-15-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 10389-65-8
di-t-butoxycarbonyl-L-cystine

: 2462-31-9
benzyl 2-aminoacetate hydrochloride

: 32381-30-9
benzyl (6R,11R)-6-((2-(benzyloxy)-2-oxoethyl)carbamoyl)-11-((tert-butoxycarbonyl)amino)-2,2-dimethyl-4,12-dioxo-3-oxa-8,9-dithia-5,13-diazapentadecan-15-oate

Guidance literature:: benzyl 2-aminoacetate hydrochloride; With 4-methyl-morpholine; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

di-t-butoxycarbonyl-L-cystine; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1.16667h;
DOI:10.1055/a-1343-5607

Reference yield:

: 1738-76-7
glycine benzyl ester p-toluenesulfonic acid salt

: 51077-22-6
N-Boc-L-cystine p-nitrophenyl ester

: 32381-30-9
benzyl (6R,11R)-6-((2-(benzyloxy)-2-oxoethyl)carbamoyl)-11-((tert-butoxycarbonyl)amino)-2,2-dimethyl-4,12-dioxo-3-oxa-8,9-dithia-5,13-diazapentadecan-15-oate

Guidance literature:: With triethylamine;

Reference yield: 91.0%

: 1-(2-(phenylethynyl)phenyl)naphthalene

: 32381-30-9
benzyl (6R,11R)-6-((2-(benzyloxy)-2-oxoethyl)carbamoyl)-11-((tert-butoxycarbonyl)amino)-2,2-dimethyl-4,12-dioxo-3-oxa-8,9-dithia-5,13-diazapentadecan-15-oate

: benzyl N-(tert-butoxycarbonyl)-S-(6-phenylbenzo[c]phenanthren-5-yl)-L-cysteinylglycinate

Guidance literature:: benzyl (6R,11R)-6-((2-(benzyloxy)-2-oxoethyl)carbamoyl)-11-((tert-butoxycarbonyl)amino)-2,2-dimethyl-4,12-dioxo-3-oxa-8,9-dithia-5,13-diazapentadecan-15-oate; With N-chloro-succinimide; In dichloromethane; at 0 ℃; for 1h;

1-(2-(phenylethynyl)phenyl)naphthalene; In dichloromethane; at 0 - 20 ℃;
DOI:10.1055/a-1343-5607