3-azido-2,4-di-O-benzyl-3-deoxy-α-D-glucopyranosyl-(1→1′)-3′-azido-2′,4′-di-O-benzyl-3′-deoxy-β-D-glucopyranoside

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Chemical Name:3-azido-2,4-di-O-benzyl-3-deoxy-α-D-glucopyranosyl-(1→1′)-3′-azido-2′,4′-di-O-benzyl-3′-deoxy-β-D-glucopyranoside
CAS No.:1430117-33-1
Molecular Formula:C₄₀H₄₄N₆O₉
Molecular Weight:752.824
Hs Code.:

Synonyms:3-azido-2,4-di-O-benzyl-3-deoxy-α-D-glucopyranosyl-(1→1′)-3′-azido-2′,4′-di-O-benzyl-3′-deoxy-β-D-glucopyranoside

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Chemical Property of 3-azido-2,4-di-O-benzyl-3-deoxy-α-D-glucopyranosyl-(1→1′)-3′-azido-2′,4′-di-O-benzyl-3′-deoxy-β-D-glucopyranoside

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Technology Process of 3-azido-2,4-di-O-benzyl-3-deoxy-α-D-glucopyranosyl-(1→1′)-3′-azido-2′,4′-di-O-benzyl-3′-deoxy-β-D-glucopyranoside

There total 1 articles about 3-azido-2,4-di-O-benzyl-3-deoxy-α-D-glucopyranosyl-(1→1′)-3′-azido-2′,4′-di-O-benzyl-3′-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1417719-93-7
6-O-acetyl-3-azido-2,4-di-O-benzyl-3-deoxy-a-D-glucopyranosyl-(1→1')-6-O-acetyl-3'-azido-2',4'-di-O-benzyl-3'-deoxy-b-D-glucopyranoside

: 1430117-33-1
3-azido-2,4-di-O-benzyl-3-deoxy-α-D-glucopyranosyl-(1→1′)-3′-azido-2′,4′-di-O-benzyl-3′-deoxy-β-D-glucopyranoside

Guidance literature:: 6-O-acetyl-3-azido-2,4-di-O-benzyl-3-deoxy-a-D-glucopyranosyl-(1→1')-6-O-acetyl-3'-azido-2',4'-di-O-benzyl-3'-deoxy-b-D-glucopyranoside; With sodium; In methanol; for 0.0833333h; Reflux; Inert atmosphere;

In methanol; Cooling;
DOI:10.1021/ja4010255

Reference yield: 71.0%

: 1430117-33-1
3-azido-2,4-di-O-benzyl-3-deoxy-α-D-glucopyranosyl-(1→1′)-3′-azido-2′,4′-di-O-benzyl-3′-deoxy-β-D-glucopyranoside

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 1430117-36-4
3-azido-2,4-di-O-benzyl-3-deoxy-6-diphenylphosphoryl-α-D-glucopyranosyl-(1→1')-3′-azido-2′,4′-di-O-benzyl-3′-deoxy-6′-diphenylphosphoryl-β-D-glucopyranoside

Guidance literature:: With dmap; In dichloromethane; at -10 ℃; Inert atmosphere;
DOI:10.1021/ja4010255

Reference yield:

: 1430117-33-1
3-azido-2,4-di-O-benzyl-3-deoxy-α-D-glucopyranosyl-(1→1′)-3′-azido-2′,4′-di-O-benzyl-3′-deoxy-β-D-glucopyranoside

: C₃₆H₄₂N₂O₁₅P₂

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / dichloromethane / -10 °C / Inert atmosphere

2: hydrazine hydrate; palladium(II) hydroxide / methanol / 16 h

3: palladium(II) hydroxide; hydrogen; acetic acid / water; methanol

With dmap; hydrogen; palladium(II) hydroxide; hydrazine hydrate; acetic acid; In methanol; dichloromethane; water;
DOI:10.1021/ja4010255