(S_S,S)-N-diphenylmethyl-2-[2-(4-isopropyl-2-thioxothiazolidin-3-yl)-2-oxo-ethylsulfinyl]acetamide

Base Information

• Chemical Name: (S_S,S)-N-diphenylmethyl-2-[2-(4-isopropyl-2-thioxothiazolidin-3-yl)-2-oxo-ethylsulfinyl]acetamide
• CAS No.: 474937-20-7
• Molecular Formula: C₂₃H₂₆N₂O₃S₃
• Molecular Weight: 474.669

Synonyms:(S_S,S)-N-diphenylmethyl-2-[2-(4-isopropyl-2-thioxothiazolidin-3-yl)-2-oxo-ethylsulfinyl]acetamide

Chemical Property of (S_S,S)-N-diphenylmethyl-2-[2-(4-isopropyl-2-thioxothiazolidin-3-yl)-2-oxo-ethylsulfinyl]acetamide

Chemical Property:

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Technology Process of (S_S,S)-N-diphenylmethyl-2-[2-(4-isopropyl-2-thioxothiazolidin-3-yl)-2-oxo-ethylsulfinyl]acetamide

There total 2 articles about (S_S,S)-N-diphenylmethyl-2-[2-(4-isopropyl-2-thioxothiazolidin-3-yl)-2-oxo-ethylsulfinyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Benzhydrylamine (91-00-9) → (SS,S)-N-diphenylmethyl-2-[2-(4-isopropyl-2-thioxothiazolidin-3-yl)-2-oxo-ethylsulfinyl]acetamide (474937-20-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 100 percent / pyridine / diethyl ether / 0.75 h / Heating

2: aq. H₂O₂ / various solvent(s) / 3 h / 20 °C

3: 72.3 mg / EDC*HCl; DMAP / CH₂Cl₂ / 1 h / 20 °C

With pyridine; dmap; dihydrogen peroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In diethyl ether; dichloromethane;

DOI:10.1248/cpb.50.558

Reference yield:

[(diphenylmethylcarbamoyl)methylsulfanyl]acetic acid (441351-66-2) → (SS,S)-N-diphenylmethyl-2-[2-(4-isopropyl-2-thioxothiazolidin-3-yl)-2-oxo-ethylsulfinyl]acetamide (474937-20-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. H₂O₂ / various solvent(s) / 3 h / 20 °C

2: 72.3 mg / EDC*HCl; DMAP / CH₂Cl₂ / 1 h / 20 °C

With dmap; dihydrogen peroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;

DOI:10.1248/cpb.50.558

Reference yield: 91.0%

sodium methylate (124-41-4) + (SS,S)-N-diphenylmethyl-2-[2-(4-isopropyl-2-thioxothiazolidin-3-yl)-2-oxo-ethylsulfinyl]acetamide (474937-20-7) → methyl(-)-(S)-[(diphenylmethylcarbamoyl)methylsulfinyl]acetate

Guidance literature:

In methanol; at 0 ℃; for 0.666667h;

DOI:10.1248/cpb.50.558

upstream raw materials:

Benzhydrylamine

[(diphenylmethylcarbamoyl)methylsulfanyl]acetic acid

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