4-(1R,2S,5R,3'S,4'S,6'S)-[5-methyl-2-(1-methyl-1-phenylethyl)-cyclohexyloxycarbonyl]-4-chlorobicyclo[2.2.1]heptene

Base Information

Chemical Name:4-(1R,2S,5R,3'S,4'S,6'S)-[5-methyl-2-(1-methyl-1-phenylethyl)-cyclohexyloxycarbonyl]-4-chlorobicyclo[2.2.1]heptene
CAS No.:211448-05-4
Molecular Formula:C₂₄H₃₁ClO₂
Molecular Weight:386.962
Hs Code.:

Synonyms:4-(1R,2S,5R,3'S,4'S,6'S)-[5-methyl-2-(1-methyl-1-phenylethyl)-cyclohexyloxycarbonyl]-4-chlorobicyclo[2.2.1]heptene

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Chemical Property of 4-(1R,2S,5R,3'S,4'S,6'S)-[5-methyl-2-(1-methyl-1-phenylethyl)-cyclohexyloxycarbonyl]-4-chlorobicyclo[2.2.1]heptene

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Technology Process of 4-(1R,2S,5R,3'S,4'S,6'S)-[5-methyl-2-(1-methyl-1-phenylethyl)-cyclohexyloxycarbonyl]-4-chlorobicyclo[2.2.1]heptene

There total 1 articles about 4-(1R,2S,5R,3'S,4'S,6'S)-[5-methyl-2-(1-methyl-1-phenylethyl)-cyclohexyloxycarbonyl]-4-chlorobicyclo[2.2.1]heptene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 141936-58-5
2-Chloro-acrylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: 211448-05-4
4-(1R,2S,5R,3'S,4'S,6'S)-[5-methyl-2-(1-methyl-1-phenylethyl)-cyclohexyloxycarbonyl]-4-chlorobicyclo[2.2.1]heptene

: 4-(1R,2S,5R,3'R,4'S,6'R)-[5-methyl-2-(1-methyl-1-phenylethyl)-cyclohexyloxycarbonyl]-4-chlorobicyclo[2.2.1]heptene

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -20 ℃; for 7h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(98)00196-7

Reference yield:

: 211448-05-4
4-(1R,2S,5R,3'S,4'S,6'S)-[5-methyl-2-(1-methyl-1-phenylethyl)-cyclohexyloxycarbonyl]-4-chlorobicyclo[2.2.1]heptene

: 95-12-5,13360-81-1,15507-06-9,42070-72-4,67505-46-8,67671-05-0,67671-06-1,69831-10-3,42070-82-6
(-)-(1S,2S,4S)-bicyclo[2.2.1]hept-5-en-2-yl methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LiAlH₄, 2.) ZnCl₂, NaBH₃CN / 1.) ether, 0 deg C, 2.) ether, reflux

2: Et₃N / CH₂Cl₂ / Ambient temperature

3: LiAlH₄ / diethyl ether / 0 °C

With lithium aluminium tetrahydride; sodium cyanoborohydride; triethylamine; zinc(II) chloride; In diethyl ether; dichloromethane;
DOI:10.1016/S0957-4166(98)00196-7

Reference yield:

: 211448-05-4
4-(1R,2S,5R,3'S,4'S,6'S)-[5-methyl-2-(1-methyl-1-phenylethyl)-cyclohexyloxycarbonyl]-4-chlorobicyclo[2.2.1]heptene

: Benzoic acid (1S,2R,4S)-1-bicyclo[2.2.1]hept-5-en-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LiAlH₄, 2.) ZnCl₂, NaBH₃CN / 1.) ether, 0 deg C, 2.) ether, reflux

2: Et₃N / CH₂Cl₂ / Ambient temperature

With lithium aluminium tetrahydride; sodium cyanoborohydride; triethylamine; zinc(II) chloride; In dichloromethane;
DOI:10.1016/S0957-4166(98)00196-7