(S)-4,4,5,5-tetramethyl-2-[6-benzoyloxy-1-hexen-3-yl]-1,3,2-dioxaborolane

Base Information

• Chemical Name: (S)-4,4,5,5-tetramethyl-2-[6-benzoyloxy-1-hexen-3-yl]-1,3,2-dioxaborolane
• CAS No.: 1000376-30-6
• Molecular Formula: C₁₉H₂₇BO₄
• Molecular Weight: 330.232

Synonyms:(S)-4,4,5,5-tetramethyl-2-[6-benzoyloxy-1-hexen-3-yl]-1,3,2-dioxaborolane

Chemical Property of (S)-4,4,5,5-tetramethyl-2-[6-benzoyloxy-1-hexen-3-yl]-1,3,2-dioxaborolane

Chemical Property:

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Technology Process of (S)-4,4,5,5-tetramethyl-2-[6-benzoyloxy-1-hexen-3-yl]-1,3,2-dioxaborolane

There total 2 articles about (S)-4,4,5,5-tetramethyl-2-[6-benzoyloxy-1-hexen-3-yl]-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

(Z)-6-benzoyloxy-2-hexen-1-yl methyl carbonate (1000376-23-7) + bis(pinacol)diborane (73183-34-3) → (S)-4,4,5,5-tetramethyl-2-[6-benzoyloxy-1-hexen-3-yl]-1,3,2-dioxaborolane (1000376-30-6)

Guidance literature:

With copper (I) tert-butoxide; In tetrahydrofuran; 0°C, 48 h;

DOI:10.1021/ja076634o

Reference yield:

(Z)-6-benzoyloxy-2-hexen-1-yl methyl carbonate (1000376-23-7) + bis(pinacol)diborane (73183-34-3) → (S)-4,4,5,5-tetramethyl-2-[6-benzoyloxy-1-hexen-3-yl]-1,3,2-dioxaborolane (1000376-30-6) + (R)-4,4,5,5-tetramethyl-2-[6-benzoyloxy-1-hexen-3-yl]-1,3,2-dioxaborolane

Guidance literature:

copper (I) tert-butoxide; In tetrahydrofuran; at 0 ℃; for 48h; Title compound not separated from byproducts.;

DOI:10.1021/ja076634o

Reference yield:

(S)-4,4,5,5-tetramethyl-2-[6-benzoyloxy-1-hexen-3-yl]-1,3,2-dioxaborolane (1000376-30-6) → (S)-4-hydroxyhex-5-en-1-yl benzoate (1000376-43-1)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide; at 0 ℃;

DOI:10.1021/ja076634o

upstream raw materials:

(Z)-6-benzoyloxy-2-hexen-1-yl methyl carbonate

bis(pinacol)diborane

Downstream raw materials:

(S)-4-hydroxyhex-5-en-1-yl benzoate

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