4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl bromide

Base Information

Chemical Name:4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl bromide
CAS No.:1338932-17-4
Molecular Formula:C₁₈H₁₂BrF₁₇
Molecular Weight:631.17
Hs Code.:

Synonyms:4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl bromide

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Chemical Property of 4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl bromide

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Technology Process of 4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl bromide

There total 1 articles about 4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1338932-15-2
4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl alcohol

: 1338932-17-4
4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl bromide

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2011.08.087

Reference yield: 88.0%

: 1338932-17-4
4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl bromide

: 582-52-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 1338932-19-6
3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-1,2:5,6-di-O-isopropylidene-α-d-glucofuranose3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

Guidance literature:: 1,2:5,6-di-O-isopropylidene-α-D-glucofuranose; With sodium hydride; In tetrahydrofuran; paraffin oil; at 0 ℃; for 0.5h; Inert atmosphere;

4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; paraffin oil; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tet.2011.08.087

Reference yield:

: 1338932-17-4
4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl bromide

: 582-52-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: C₂₄H₂₃F₁₇O₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; paraffin oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 16 h / 0 - 20 °C / Inert atmosphere

2.1: water; trifluoroacetic acid / dichloromethane / 5 h / 20 °C

With water; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; paraffin oil;
DOI:10.1016/j.tet.2011.08.087